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History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
21 19:38:59 ap.200928.a400 11 P31CPD ap - + - - - + - 7-45_2.5h
21 19:27:53 ap.200928.a400 10 PROTON ap + + - + + + + 7-45_2.5h
10 18:43:18 lbp.200928.a400 20 PROTON lbp + + - + + + + LBP-12-4-F2TO7
2 18:01:46 lbp.200928.a400 10 PROTON lbp + + - + + + + LBP-12-4-F11TO12
20 17:46:28 rg.200928.a400 20 PROTON rg + + - - + + + RGV_206 sref: reference peak not found default calibration done
19 17:39:43 rg.200928.a400 10 PROTON rg + + - + + + + RGV_205 sref: reference peak not found default calibration done
22 17:31:49 fr.200928.a400 51 COSY fr - + - - - + + FR-122-1E - COSY
22 17:24:32 fr.200928.a400 50 PROTON fr + + - + + + + FR-122-1E - HNMR sref: reference peak not found default calibration done
9 17:15:42 gb.200928.a400 20 PROTON gb + + - - + + + FILTRATO sref: reference peak not found default calibration done
15 16:45:39 naa.200928.a400 21 C13 naa - + - - - + + NAA90 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
15 16:40:16 naa.200928.a400 20 PROTON naa + + - - x + + NAA90 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
14 16:10:09 naa.200928.a400 11 C13 naa - + - - - + + NAA89 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
14 16:02:53 naa.200928.a400 10 PROTON naa + + - + + + + NAA89
8 14:56:43 mmsh.200928.a400 22 C13 mmsh - + - - - + + TS2O au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 14:50:53 mmsh.200928.a400 21 COSY mmsh - + - - - + + TS2O
8 14:43:53 mmsh.200928.a400 20 PROTON mmsh + + - + + + + TS2O sref: reference peak not found default calibration done
22 14:35:58 fr.200928.a400 40 PROTON fr + + - + + + + FR-122-1B D2O SALT sref: reference peak not found default calibration done; pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of E:/current_data/data/fr/nmr/fr.200928.a400/40/pdata/1/peaks!
5 14:27:51 gb.200928.a400 10 PROTON gb + + - + + + + GB-DIMAMPROT-CRUDE
8 14:19:43 mmsh.200928.a400 10 PROTON mmsh + + - + + + + MH01-TSO2-2 sref: reference peak not found default calibration done
22 14:10:21 fr.200928.a400 30 PROTON fr + + - + + + + FR-122-1B - HNMR SAMPLE 2 sref: reference peak not found default calibration done
1 13:54:21 krb.200928.a400 11 C13 krb - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 13:46:42 krb.200928.a400 10 PROTON krb + + - + + + +
13 13:39:25 av.200928.a400 10 PROTON av + + - + + + + 2-01
22 13:12:20 fr.200928.a400 21 COSY fr - + - - - + + FR-122-1B COSY
22 13:04:00 fr.200928.a400 20 PROTON fr + + - + + + + FR-122-1B - HNMR sref: reference peak not found default calibration done
10 11:50:37 fr.200928.a400 11 PROTON fr - + - - - + + FR-119-1i - HNMR
10 11:43:44 fr.200928.a400 10 PROTON fr + + - + + + + FR-119-1i - HNMR
4 11:17:34 aog_011_Aq.200928.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
7 10:36:08 kd.200928.a400 20 PROTON kd + + - - + + + 5g, tube 2
6 10:29:01 kd.200928.a400 10 PROTON kd + + - + + + + 5g, tube 1
3 09:45:47 aog_011_W.200928.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
23 20:27:32 ap.200927.a400 21 P31CPD ap - + - - - + + 7-44
23 20:16:27 ap.200927.a400 20 PROTON ap + + - + + + + 7-44
14 16:02:56 ap.200927.a400 11 P31CPD ap - + - - - + + 7-36, 40, 42_together
14 15:51:55 ap.200927.a400 10 PROTON ap + + - + + + + 7-36, 40, 42_together
22 03:48:49 ap.200925.a400 51 P31CPD ap - + - - - + + 7-41_F0
22 03:31:43 ap.200925.a400 50 PROTON ap + + - - + + + 7-41_F0
21 02:31:42 ap.200925.a400 42 C13CPD ap - + - - - + + 7-41_F2 sref: reference peak not found default calibration done
21 02:29:34 ap.200925.a400 41 P31CPD ap - + - - - + + 7-41_F2
21 02:18:06 ap.200925.a400 40 PROTON ap + + - + + + + 7-41_F2
19 01:15:05 lbp.200925.a400 31 C13APT_KU_night lbp + + - - + + + LBP-12-2-F16-26 sref: reference peak not found default calibration done
18 00:13:43 lbp.200925.a400 21 C13APT_KU_night lbp + + - - x + + LBP-12-2-F8to14 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
12 22:08:58 krb.200925.a400 20 C13CPD krb + + - + + + + sref: reference peak not found default calibration done
20 22:07:02 ap.200925.a400 31 P31CPD ap - + - - - + + 7-41_F1
20 21:55:27 ap.200925.a400 30 PROTON ap + + - + + + + 7-41_F1
15 20:30:50 ap.200925.a400 21 P31CPD ap - + - - - + + 7-42
15 20:18:52 ap.200925.a400 20 PROTON ap + + - + + + + 7-42
24 19:52:47 yd.200925.a400 30 PROTON yd + + - - + + + YD-507-B
23 19:47:29 yd.200925.a400 20 PROTON yd + + - - x + + YD-507-A topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
22 19:39:45 yd.200925.a400 10 PROTON yd + + - + + + + YD-512-214-pure
21 18:29:23 pd.200925.a400 40 PROTON pd + + - - + + + PD-236-CR_CD3CN
20 18:27:08 pd.200925.a400 31 P31CPD pd - + - - - + + PD228-CR_CD3CN
20 18:20:10 pd.200925.a400 30 PROTON pd + + - + + + + PD228-CR_CD3CN
19 18:03:20 lbp.200925.a400 30 PROTON lbp + + - - + + + LBP-12-2-F16-26
18 17:55:27 lbp.200925.a400 20 PROTON lbp + + - + + + + LBP-12-2-F8to14
13 16:23:27 bhg662_conc.200925.a400 10 Quant_KU bhg + + - + + + + pulsecal: setting option 'sn' for organic solvent (DMSO)
17 15:37:12 ye_43B_0.200925.a400 10 PROTON ye + + - + + + + sref: reference peak not found default calibration done
13 15:19:27 bhgJAN004_co.200925.a400 10 Quant_KU bhg + + - + + + + pulsecal: setting option 'sn' for organic solvent (DMSO), sref: reference peak not found default calibration done
15 14:57:57 cvh.200925.a400 11 C13 cvh + + - + + + + CVI1-72 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done; pp: Unable to assign a peak for scaling of E:/current_data/data/cvh/nmr/cvh.200925.a400/11/pdata/1/peaks No peak is found in the specified ranges!
15 14:33:13 cvh.200925.a400 10 PROTON cvh + + - + + + + CVI1-72
8 14:27:08 pd.200925.a400 22 PROTON pd - + - - - + + PD-270-CR_12h
8 14:25:14 pd.200925.a400 21 P31CPD pd - + - - - + + PD-270-CR_12h
8 14:18:52 pd.200925.a400 20 P31CPD pd + + - + + + + PD-270-CR_12h
4 13:37:48 krb.200925.a400 12 F19CPD_KU krb + + - + + + +
16 13:35:40 ap.200925.a400 11 P31CPD ap - + - - - + + 7-40
16 13:24:18 ap.200925.a400 10 PROTON ap + + - + + + + 7-40
6 13:22:05 pd.200925.a400 11 P31CPD pd - + - - - + + PD-268_1_12h
6 13:13:06 pd.200925.a400 10 PROTON pd + + - + + + + PD-268_1_12h
4 12:00:12 krb.200925.a400 11 C13 krb + + - - + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 11:44:28 ki.200925.a400 11 C13 ki - + - - - + + LBP-12-2-AE au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 11:35:42 ki.200925.a400 10 PROTON ki + + - + + + + LBP-12-2-AE
5 11:29:18 ki514_3.200925.a400 10 PROTON ki + + - + + + + KI 514-3 sref: reference peak not found default calibration done
4 11:12:36 krb.200925.a400 10 PROTON krb + + - + + + +
10 10:41:01 lbp.200925.a400 10 PROTON lbp + + - + + + + LBP-12-2-crude
7 09:35:02 slb.200925.a400 11 C13APT_KU slb - + - - - + + SLB_71 ax au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
7 09:28:06 slb.200925.a400 10 PROTON slb + + - + + + + SLB_71 ax
1 09:00:18 ms096rc.200925.a400 11 F19_KU ms - + - - - + + MS1061-096 18h DS
1 08:53:14 ms096rc.200925.a400 10 PROTON ms + + - + + + + MS1061-096 18h DS sref: reference peak not found default calibration done
24 02:38:42 ap.200924.a400 34 P31CPD ap - + - - - + + 6-48 & Eu(famac)3
24 01:32:46 ap.200924.a400 33 C13CPD ap + + - + + + + 6-48 & Eu(famac)3 sref: reference peak not found default calibration done
6 00:26:44 jgl.200924.a400 11 C13CPD jgl + + - + + + + Javier Garcia JGL01 pure sref: reference peak not found default calibration done
7 00:20:58 tej.200924.a400 13 COSY tej - + - - - + + lbk 001
7 00:05:15 tej.200924.a400 14 HSQC tej - + - - - + + lbk 001
7 00:02:43 tej.200924.a400 12 F19CPD_KU tej - + - - - + + lbk 001
7 22:00:05 tej.200924.a400 11 C13CPD tej + + - + + + + lbk 001 sref: reference peak not found default calibration done
20 21:11:34 ap.200924.a400 41 P31CPD ap - + - - - + + 7-41_crude
20 21:00:35 ap.200924.a400 40 PROTON ap + + - + + + + 7-41_crude
24 20:25:10 ap.200924.a400 32 F19CPD_KU ap - + - - - + + 6-48 & Eu(famac)3
24 20:22:57 ap.200924.a400 31 P31CPD ap - + - - - + + 6-48 & Eu(famac)3
24 20:11:39 ap.200924.a400 30 PROTON ap + + - + + + + 6-48 & Eu(famac)3
17 19:39:40 yd.200924.a400 40 PROTON yd + + - - x + + YD-510-212-Pure-A topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
16 19:32:30 yd.200924.a400 30 PROTON yd + + - - + + + YD-510-212-Pure B
13 19:02:24 pd.200924.a400 22 C13 pd - + - - - + + PD-228_30 days au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
13 19:00:08 pd.200924.a400 21 P31CPD pd - + - - - + + PD-228_30 days
13 18:53:05 pd.200924.a400 20 PROTON pd + + - + + + + PD-228_30 days sref: reference peak not found default calibration done
12 18:41:59 gg.200924.a400 20 PROTON gg + + - + + + + GG01-122_Organic_Layer sref: reference peak not found default calibration done
10 18:39:30 ap.200924.a400 21 F19CPD_KU ap - + - - - + + Eu(famac)3
10 18:28:17 ap.200924.a400 20 PROTON ap + + - + + + + Eu(famac)3
22 18:01:36 kd.200924.a400 20 PROTON kd + + - - + + + Ether phase sref: reference peak not found default calibration done
21 17:53:25 kd.200924.a400 10 PROTON kd + + - + + + + starting material sref: reference peak not found default calibration done
15 17:02:20 slb.200924.a400 20 C13APT_KU slb + + - + + + + SLB_71 eq au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
12 16:29:34 gg.200924.a400 10 PROTON gg + + - + + + + GG01-124_1st_step sref: reference peak not found default calibration done
9 15:55:00 pd.200924.a400 11 P31CPD pd - + - - - + + PD3-269-CR
9 15:48:08 pd.200924.a400 10 PROTON pd + + - + + + + PD3-269-CR
6 15:30:50 jgl.200924.a400 10 PROTON jgl + + - - + + + Javier Garcia JGL01 pure
24 15:15:21 slb.200924.a400 11 C13APT_KU slb - + - - - + + SLB_71 eq au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
24 15:07:58 slb.200924.a400 10 PROTON slb + + - + + + + SLB_71 eq
20 14:55:09 krb.200924.a400 10 PROTON krb + + - - + + +
11 14:49:20 kb.200924.a400 11 COSY kb - + - - - + + KBCL112 flash tubes 1-5
11 14:37:51 kb.200924.a400 10 PROTON kb + + - - + + + KBCL112 flash tubes 1-5
2 14:22:05 mef.200924.a400 11 C13 mef - + - - - + + NAA88_PURE au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 14:13:22 mef.200924.a400 10 PROTON mef + + - - + + + NAA88_PURE
16 14:06:29 yd.200924.a400 10 PROTON yd + + - - + + + YD-509-211-pure
18 13:59:06 cvh.200924.a400 10 PROTON cvh + + - + + + + CVI1-74
15 13:50:57 ms097.200924.a400 10 PROTON ms + + - + + + + MS1062-097
8 13:15:39 aog_010_Aq2C.200924.a400 10 C13 aog + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 12:59:36 lbp.200924.a400 11 C13 lbp - + - - - + + LBP-12-1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 12:50:17 lbp.200924.a400 10 PROTON lbp + + - + + + + LBP-12-1
9 12:44:09 cyl.200924.a400 20 PROTON cyl + + - - + + + MCD_CL-02-71-2F sref: reference peak not found default calibration done
7 12:37:40 tej.200924.a400 10 PROTON tej + + - - + + + lbk 001 sref: reference peak not found default calibration done
1 12:27:52 aog.200924.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
3 11:37:39 gb.200924.a400 10 PROTON gb + + - + + + + GB-NITROPYAP sref: reference peak not found default calibration done
5 11:19:12 cv.200924.a400 10 PROTON cv + + - + + + + CV_ctrl_lactic acid sigma sref: reference peak not found default calibration done
6 10:16:39 ap.200924.a400 11 P31CPD ap - + - - - + + 7-39_2d in MeOD
6 10:04:38 ap.200924.a400 10 PROTON ap + + - + + + + 7-39_2d in MeOD zg: Error in ipsoControl::checkStatus(): Status line active!, Error in Master: Error 112 in SGU2: -- SLOT 5 RACK 1: SGU2 AD SLOT 5 RACK 1: SBSB Wake-Up occured during acquisition, SGU CPU reboot
14 09:57:51 ki514_3.200924.a400 10 PROTON ki + + - + + + + KI 514-3 sref: reference peak not found default calibration done
13 09:04:08 cyl.200924.a400 10 PROTON cyl + + - + + + + MCD_CL-02-72 sref: reference peak not found default calibration done
10 23:20:51 pd.200923.a400 42 C13CPD pd + + - + + + + PD-268-CR_2
14 23:05:26 em1046p.200923.a400 12 HSQC emr - + - - - + +
14 22:00:16 em1046p.200923.a400 11 C13CPD emr + + - + + + + sref: reference peak not found default calibration done
22 20:35:46 cv.200923.a400 80 PROTON cv + + - - + + + Stabiliy 2M 37 95/50 sref: reference peak not found default calibration done
21 20:19:43 cv.200923.a400 70 PROTON cv + + - - + + + Stabiliy 2M 37 95/5 sref: reference peak not found default calibration done
20 20:03:46 cv.200923.a400 60 PROTON cv + + - - + + + Stabiliy 2M RT 95/50 sref: reference peak not found default calibration done
19 19:47:29 cv.200923.a400 50 PROTON cv + + - - + + + Stabiliy 2M RT 95/5 sref: reference peak not found default calibration done
18 19:31:30 cv.200923.a400 40 PROTON cv + + - - + + + Stabiliy 2M 4C 95/50 sref: reference peak not found default calibration done
17 19:14:38 cv.200923.a400 30 PROTON cv + + - + + + + Stabiliy 2M 4C 95/5 sref: reference peak not found default calibration done
9 19:12:43 pd.200923.a400 51 P31CPD pd - + - - - + + PD-269_TBHP_2h
9 19:05:18 pd.200923.a400 50 PROTON pd + + - + + + + PD-269_TBHP_2h
1 18:58:01 yd.200923.a400 10 PROTON yd + + - + + + + YD-600-204-water phase in D2O sref: reference peak not found default calibration done
5 18:42:00 jiz.200923.a400 10 PROTON jiz + + - - + + + UCAB#792_2 sref: reference peak not found default calibration done
4 18:35:01 cyl.200923.a400 20 PROTON cyl + + - + + + + CL_02_70 sref: reference peak not found default calibration done
12 18:27:04 kd.200923.a400 10 PROTON kd + + - + + + + compound 4, pure
10 18:24:50 pd.200923.a400 41 P31CPD pd - + - - - + + PD-268-CR_2
10 18:17:18 pd.200923.a400 40 PROTON pd + + - + + + + PD-268-CR_2
16 18:01:43 cv.200923.a400 20 PROTON cv + + - - + + + CV004 z10atto665 230920 sref: reference peak not found default calibration done
15 17:44:50 cv.200923.a400 10 PROTON cv + + - + + + + CV063 95/50 atto665 230920 sref: reference peak not found default calibration done
24 17:42:46 jcmh.200923.a400P3P2 12 F19CPD_KU jcmh - + - - - + +
24 17:40:54 jcmh.200923.a400P3P2 11 F19_KU jcmh - + - - - + +
24 17:33:21 jcmh.200923.a400P3P2 10 PROTON jcmh + + - - + + + sref: reference peak not found default calibration done
23 17:31:12 jcmh.200923.a400P3P1 12 F19CPD_KU jcmh - + - - - + +
23 17:28:51 jcmh.200923.a400P3P1 11 F19_KU jcmh - + - - - + +
23 17:20:41 jcmh.200923.a400P3P1 10 PROTON jcmh + + - + + + + sref: reference peak not found default calibration done
8 16:46:11 aog_004_C.200923.a400 10 C13 aog + + - - + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 16:19:26 aog_009_Aq2.200923.a400 11 C13 aog - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 16:09:45 aog_009_Aq2.200923.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
6 15:40:55 gb.200923.a400 10 PROTON gb + + - + + + + GB-NITROPYAP-1
18 15:39:00 mef.200923.a400 21 F19_KU mef - + - - - + + MEF96_3-I_pure sref: reference peak outside file limits default calibration done
18 15:30:10 mef.200923.a400 20 PROTON mef + + - - + + + MEF96_3-I_pure sref: reference peak not found default calibration done
19 15:27:59 mef.200923.a400 11 F19_KU mef - + - - - + + MEF70_2-I_pure sref: reference peak outside file limits default calibration done
19 15:19:00 mef.200923.a400 10 PROTON mef + + - + + + + MEF70_2-I_pure sref: reference peak not found default calibration done
3 15:09:01 aog_009_Aq.200923.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
1 14:46:27 krb.200923.a400 20 C13 krb + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 14:44:20 pd.200923.a400 31 P31CPD pd - + - - - + + PD-268-CR_1
5 14:37:27 pd.200923.a400 30 PROTON pd + + - + + + + PD-268-CR_1
4 14:21:40 krb.200923.a400 10 PROTON krb + + - - + + +
14 14:14:11 em1046p.200923.a400 10 PROTON emr + + - - + + +
9 13:58:29 lbp.200923.a400 11 C13 lbp - + - - - + + LPB-SM2 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
9 13:52:45 lbp.200923.a400 10 PROTON lbp + + - - x + + LPB-SM2 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
17 13:16:37 civ.200923.a400 20 C13 civ + + - + + + + CIV1-12-B au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
22 13:01:24 cvh.200923.a400 20 PROTON cvh + + - + + + + CVI1-73 20-22
20 12:53:41 cyl.200923.a400 10 PROTON cyl + + - + + + + mcd_cl-02-68 sref: reference peak not found default calibration done
16 12:15:42 civ.200923.a400 11 C13 civ - + - - - + + CIV1-12-B au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
16 12:06:43 civ.200923.a400 10 PROTON civ + + - + + + + CIV1-12-B
13 11:52:35 ki514_2.200923.a400 10 PROTON ki + + - + + + + KI 514-2 sref: reference peak not found default calibration done
12 10:56:21 pd.200923.a400 20 P31CPD pd + + - + + + + PD-268-CR
10 10:49:06 cvh.200923.a400 10 PROTON cvh + + - + + + + CVI1-73
7 10:39:53 ap.200923.a400 11 P31CPD ap - + - - - + + AP-7-39
7 10:32:08 ap.200923.a400 10 PROTON ap + + - + + + + AP-7-39
5 10:30:01 pd.200923.a400 13 P31CPD ap - + - - - + +
5 09:59:56 pd.200923.a400 12 C13 pd - + - - - + + PD-268-CR au_zg_max30min: --- au_zg_max30min finished ---
5 09:57:45 pd.200923.a400 11 P31CPD pd - + - - - + + PD-268-CR
5 09:50:31 pd.200923.a400 10 PROTON pd + + - + + + + PD-268-CR
5 03:05:10 mef.200922.a400 30 C13CPD mef + + - + + + + MEF97_PURE sref: reference peak not found default calibration done
21 23:04:42 cbc.200922.a400 24 C13CPD cbc + + - + + + + CBC014 peak 2 prep sref: reference peak not found default calibration done
11 22:00:11 rg.200922.a400 21 C13CPD rg + + - + + + + RGV_203 sref: reference peak not found default calibration done
12 19:24:06 yd.200922.a400 50 PROTON yd + + - + + + + YD-600-204-pure
11 17:13:41 rg.200922.a400 20 PROTON rg + + - - + + + RGV_203 sref: reference peak not found default calibration done
6 17:06:51 yd.200922.a400 40 PROTON yd + + - + + + + YD-600-197-white solid- washed with acetone sref: reference peak not found default calibration done
7 15:50:58 ms.200922.a400 11 COSY ms - + - - - + + POTz 2 crude
7 15:43:50 ms.200922.a400 10 PROTON ms + + - + + + + POTz 2 crude
5 14:54:05 mef.200922.a400 21 C13 mef - + - - - + + MEF97_pure au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 14:47:07 mef.200922.a400 20 PROTON mef + + - + + + + MEF97_pure sref: reference peak not found default calibration done
6 14:45:53 mef.200922.a400 10 PROTON mef x - - - - - - MEF97_PUR Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 6
10 14:29:23 cvh.200922.a400 10 PROTON cvh + + - - + + + CVI1-72 11-13
9 14:21:46 kd.200922.a400 10 PROTON kd + + - - + + + compound 4, 0.5 g
8 14:14:12 aw4_27_1.200922.a400 10 PROTON aw + + - + + + + AW4-27-1 crude rxn after work up sref: reference peak not found default calibration done
7 13:58:38 aw4_31_1.200922.a400 11 C13 aw - + - - - + + AW4-31-1 sub2 rgt3 30 min au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
7 13:50:21 aw4_31_1.200922.a400 10 PROTON aw + + - + + + + AW4-31-1 sub2 rgt3 30 min sref: reference peak not found default calibration done
3 12:42:23 yd.200922.a400 30 PROTON yd + + - + + + + YD-510-208-water phase in D2O sref: reference peak not found default calibration done
2 12:35:45 yd.200922.a400 20 PROTON yd + + - + + + + YD-510-208-white solid washed with heptane sref: reference peak not found default calibration done
1 12:34:11 yd.200922.a400 10 PROTON yd x - - - - - - YD-510-208-white solid Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 1
24 12:00:34 rg.200922.a400 11 PROTON rg - + - - - + + RGV_203 sref: reference peak not found default calibration done
24 11:54:15 rg.200922.a400 10 PROTON rg + + - + + + + RGV_203 sref: reference peak not found default calibration done
21 11:27:23 cbc.200922.a400 23 HSQC cbc + + - + + + + CBC014 peak 2 prep
13 11:18:20 krb.200922.a400 10 PROTON krb + + - + + + +
21 11:15:30 cbc.200922.a400 22 F19CPD_KU cbc - + - - - + + CBC014 peak 2 prep
21 11:09:40 cbc.200922.a400 21 COSY cbc - + - - - + + CBC014 peak 2 prep
21 10:59:11 cbc.200922.a400 20 PROTON cbc + + - - + + + CBC014 peak 2 prep
20 10:48:11 cbc.200922.a400 10 PROTON cbc + + - + + + + CPO903 check
18 09:49:44 gg.200922.a400 10 PROTON gg + + - + + + + GG01-116_FDR sref: reference peak not found default calibration done
14 09:39:36 rr.200922.a400 50 PROTON rr + + - - + + + 175
13 09:33:42 rr.200922.a400 40 PROTON rr + + - - + + + 173
12 09:26:35 rr.200922.a400 30 PROTON rr + + - + + + + 172
16 09:19:28 aw4_26.200922.a400 10 PROTON aw + + - + + + + AW4-26 crude over night rxn
11 09:13:10 rr.200922.a400 20 PROTON rr + + - - + + + 171
10 09:06:29 rr.200922.a400 10 PROTON rr + + - + + + + 170
8 02:29:41 ki533_1.200921.a400 11 C13CPD ki + + - - + + + KI 533-1 sref: reference peak not found default calibration done
7 01:25:01 ki514_2.200921.a400 11 C13CPD ki + + - + + + + KI 514-2 sref: reference peak not found default calibration done
6 00:19:24 krb.200921.a400 30 C13CPD krb + + - + + + + sref: reference peak not found default calibration done
3 23:49:54 aog_005.200921.a400 13 HSQC aog - + - - - + +
3 23:04:11 aog_005.200921.a400 12 HMBC aog - + - - - + +
3 22:00:06 aog_005.200921.a400 11 C13CPD aog + + - + + + + sref: reference peak not found default calibration done
22 20:36:34 ap.200921.a400 81 P31CPD ap - + - - - + + 7-39
22 20:25:17 ap.200921.a400 80 PROTON ap + + - + + + + 7-39
11 19:24:11 ap.200921.a400 70 PROTON ap + + - + + + + Eu(famac)3
13 19:21:59 ap.200921.a400 51 F19CPD_KU ap - + - - - + + Eu(famac)3
13 19:10:02 ap.200921.a400 50 PROTON ap + + - + + + + Eu(famac)3
23 18:47:43 gb.200921.a400 20 PROTON gb + + - + + + + GB-19-CRUDE
12 18:33:00 ap.200921.a400 41 F19CPD_KU ap - + - - - + + Eu reagent chiral shift
12 18:22:14 ap.200921.a400 40 PROTON ap + + - + + + + Eu reagent chiral shift
24 18:01:07 gb.200921.a400 10 PROTON gb + + - + + + + GB-19
10 16:03:58 par.200921.a400 10 PROTON par + + - + + + + 105-003-C
21 15:51:13 cyl.200921.a400 10 PROTON cyl + + - + + + + MCD_CL-02-66 sref: reference peak not found default calibration done
17 15:02:32 ap.200921.a400 31 P31CPD ap - + - - - + + 7-38
17 14:51:16 ap.200921.a400 30 PROTON ap + + - + + + + 7-38
5 14:25:47 cvh.200921.a400 20 PROTON cvh + + - + + + + CVH1-12
2 13:52:03 aog_007.200921.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
20 13:49:49 ap.200921.a400 21 P31CPD ap - + - - - + + 7-38_3h
20 13:38:32 ap.200921.a400 20 PROTON ap + + - + + + + 7-38_3h
8 13:07:11 ki533_1.200921.a400 10 PROTON ki + + - - + + + KI 533-1 sref: reference peak not found default calibration done
7 12:59:22 ki514_2.200921.a400 10 PROTON ki + + - + + + + KI 514-2 sref: reference peak not found default calibration done
16 12:29:18 pd.200921.a400 11 C13 pd - + - - - + + PD-266A_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
16 12:20:46 pd.200921.a400 10 PROTON pd + + - + + + + PD-266A_1
1 12:14:01 aog_006_2.200921.a400 10 PROTON aog + + - - + + + sref: reference peak not found default calibration done
20 12:05:41 ial_42_1.200921.a400 10 PROTON ial + + - + + + + sref: reference peak not found default calibration done
18 11:58:28 _BioOrg.200921.a400 70 PROTON _BioOrg + + - - + + + Hold 2 Projekt 6 Pent-4-enyl-2,3,4,6-tetra-O-acetyl-beta-D-Glcp
17 11:50:45 _BioOrg.200921.a400 60 PROTON _BioOrg + + - - + + + Hold 2 Projekt 6 Skab 95 Penyl 2,3,4,6-tetra-O-acetyl-beta-D-Glcp (-1-thio-)?
14 11:43:21 _BioOrg.200921.a400 50 PROTON _BioOrg + + - - + + + Hold 2 Projekt 4 skab 68 ? Boc-Ala-Phe-OMe
13 11:35:43 _BioOrg.200921.a400 40 PROTON _BioOrg + + - - + + + Hold 2 Projekt 1 Boc-Ala-Phe-OMe
12 11:28:21 _BioOrg.200921.a400 30 PROTON _BioOrg + + - - + + + Hold 1 Projekt 6 Skab 26 Thioglycosid
11 11:21:04 _BioOrg.200921.a400 20 PROTON _BioOrg + + - - + + + Hold 1 Projekt 4 Skab 45 Boc-Ala-Phe-OMe
10 11:13:44 _BioOrg.200921.a400 10 PROTON _BioOrg + + - - + + + Hold 1 Projekt 3 Boc-Phe-Ala-OMe
9 11:05:40 cvh.200921.a400 10 PROTON cvh + + - - + + + CVI1-63
15 10:44:53 krb.200921.a400 20 C13 krb + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
3 10:26:05 aog_005.200921.a400 10 PROTON aog + + - - + + + sref: reference peak not found default calibration done
4 10:15:40 aog_006.200921.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
16 10:07:22 krb.200921.a400 10 PROTON krb + + - + + + +
19 10:05:27 ap.200921.a400 11 P31CPD ap - + - - - + + 7-37b_1d in MeOD
19 09:54:13 ap.200921.a400 10 PROTON ap + + - + + + + 7-37b_1d in MeOD
7 21:06:36 ap.200920.a400 31 P31CPD ap - + - - - + + 7-37_b
7 20:55:22 ap.200920.a400 30 PROTON ap + + - + + + + 7-37_b sref: reference peak not found default calibration done
6 20:53:24 ap.200920.a400 21 P31CPD ap - + - - - + + 7-37_a
6 20:42:31 ap.200920.a400 20 PROTON ap + + - + + + + 7-37_a
24 12:42:45 ap.200920.a400 11 P31CPD ap - + - - - + + 7-36_after 1d in MeOD
24 12:31:18 ap.200920.a400 10 PROTON ap + + - + + + + 7-36_after 1d in MeOD
12 11:52:17 cvh.200920.a400 10 PROTON cvh + + - + + + + CVI1-71
15 15:27:05 cvh.200919.a400 10 PROTON cvh + + - + + + + CVI1-70
10 22:00:45 naa.200918.a400 30 C13CPD naa + + - + + + + NAA83 sref: reference peak not found default calibration done
24 21:41:10 ap.200918.a400 31 P31CPD ap - + - - - + + 7-36
24 21:30:21 ap.200918.a400 30 PROTON ap + + - + + + + 7-36
18 19:09:27 at2odwro.200918.a400 10 PROTON at + + - - + + + sref: reference peak not found default calibration done
17 19:02:05 atdwro.200918.a400 10 PROTON at + + - + + + + sref: reference peak not found default calibration done
9 18:30:51 at.200918.a400 10 PROTON at + + - + + + + sref: reference peak not found default calibration done
14 18:12:30 atble.200918.a400 10 PROTON at + + - - + + +
13 18:04:39 atprasino.200918.a400 10 PROTON at + + - - + + +
19 17:56:48 atteliko.200918.a400 10 PROTON at + + - + + + +
1 17:36:48 mef.200918.a400 11 F19CPD_KU mef - + - - - + + MEF98_pure_19F sref: reference peak outside file limits default calibration done
1 17:28:42 mef.200918.a400 10 F19_KU mef + + - + + + + MEF98_pure_19F sref: reference peak outside file limits default calibration done
11 17:22:19 ap.200918.a400 21 PROTON ap - + - - - + + 7-36_5h
11 17:15:08 ap.200918.a400 20 P31CPD ap + + - + + + + 7-36_5h
5 17:07:58 yd.200918.a400 20 PROTON yd + + - - + + + YD-509-206-fraction 11-17
4 17:01:06 yd.200918.a400 10 PROTON yd + + - + + + + YD-509-206-fraction 7-10
23 15:52:28 ap.200918.a400 10 P31CPD ap + + - + + + + 7-23_F1
6 15:40:21 fr.200918.a400 40 PROTON fr + + - - + + + FR-119-1G - HNMR
12 15:19:21 pd.200918.a400 11 C13 pd + + - + + + + PD-266A au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 14:44:43 naa.200918.a400 20 C13 naa + + - - + + + NAA83-impure au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
20 14:29:00 lbp.200918.a400 11 C13 lbp - + - - - + + LBP-3-2-afterextraction au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
20 14:21:26 lbp.200918.a400 10 PROTON lbp + + - + + + + LBP-3-2-afterextraction sref: reference peak not found default calibration done
16 13:41:15 cyl.200918.a400 10 PROTON cyl + + - + + + + mcd_cl-L-1 sref: reference peak not found default calibration done
12 13:10:38 pd.200918.a400 10 PROTON pd + + - + + + + PD-266A sref: reference peak not found default calibration done
10 12:44:38 naa.200918.a400 11 C13 naa - + - - - + + NAA83-impure au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 12:37:46 naa.200918.a400 10 PROTON naa + + - + + + + NAA83-impure sref: reference peak not found default calibration done
20 12:26:25 fr.200918.a400 30 PROTON fr + + - + + + + FR-121-1B - HNMR
22 11:22:22 fr.200918.a400 20 PROTON fr + + - - + + + 2-PYRROLIDIDONE
21 11:15:08 fr.200918.a400 10 PROTON fr + + - + + + + FR-121-1A - HNMR
3 09:58:40 aog_008_P2.200918.a400 10 PROTON aog + + - - + + + sref: reference peak not found default calibration done
2 09:49:25 aog_008_E.200918.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
1 08:59:16 ays.200918.a400 10 PROTON ays + + - + + + + FmocHN-Gly-Glycolic acid sref: reference peak not found default calibration done
13 20:19:42 ap.200917.a400 41 P31CPD ap - + - - - + + 7-35_b_5.5h
13 20:08:45 ap.200917.a400 40 PROTON ap + + - + + + + 7-35_b_5.5h
24 19:48:28 pd.200917.a400 11 P31CPD pd - + - - - + + PD-260A pp: Cannot find any peak for scaling in E:/current_data/data/pd/nmr/pd.200917.a400/11/pdata/1/peaks!
24 19:37:52 pd.200917.a400 10 PROTON pd + + - - + + + PD-260A
21 19:31:28 ap.200917.a400 31 PROTON ap - + - - - + + 7-35b_5h
21 19:24:29 ap.200917.a400 30 P31CPD ap + + - + + + + 7-35b_5h
18 18:21:24 ap.200917.a400 21 P31CPD ap - + - - - + + 7-35b_4h
18 18:10:22 ap.200917.a400 20 PROTON ap + + - + + + + 7-35b_4h
8 17:15:19 slb.200917.a400 50 PROTON slb + + - - + + + SLB71 eq F14-15
7 17:08:49 slb.200917.a400 40 PROTON slb + + - - + + + SLB_71 eq F11-13
6 17:01:59 slb.200917.a400 30 PROTON slb + + - - + + + SLB_71 eq F7-10
5 16:55:13 slb.200917.a400 20 PROTON slb + + - - + + + SLB_71 ax F7-18
4 16:47:58 slb.200917.a400 10 PROTON slb + + - + + + + SLB_71 F2-4
15 16:21:12 cvh.200917.a400 30 PROTON cvh + + - - + + + CVI1-63
17 16:14:22 cbc.200917.a400 20 PROTON cbc + + - + + + + CBC143 yellow oil (product)
16 16:11:57 cbc.200917.a400 11 B11_KU cbc - + - - - + + CBC143 white semi-solid pp: Cannot find the scaling regions file! It cannot be used for peak assignment for scaling of E:/current_data/data/cbc/nmr/cbc.200917.a400/11/pdata/1/peaks!
16 16:04:55 cbc.200917.a400 10 WATER cbc + + - + + + + CBC143 white semi-solid sref: reference peak not found default calibration done, sref: reference peak not found default calibration done
12 15:33:14 ap.200917.a400 11 P31CPD ap - + - - - + + 7-35a
12 15:22:31 ap.200917.a400 10 PROTON ap + + - + + + + 7-35a
1 14:13:02 krb.200917.a400 10 PROTON krb + + - + + + +
3 13:23:18 aog_008_S_2.200917.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
15 11:46:54 cvh.200917.a400 20 PROTON cvh + + - + + + + CVI1-20
10 10:21:25 cvh.200917.a400 11 C13 cvh + + - + + + + CVI1-69 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 10:04:59 cpo.200916.a400 16 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check - 24h sref: reference peak not found default calibration done
10 09:57:12 cvh.200917.a400 10 PROTON cvh + + - + + + + CVI1-69
19 23:33:29 mci2ex5f1218.200916.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
21 23:31:30 ap.200916.a400 41 P31CPD ap - + - - - + + 7-30_3rd FCC_F3
21 23:20:31 ap.200916.a400 40 PROTON ap + + - - + + + 7-30_3rd FCC_F3
18 23:13:55 ap.200916.a400 31 P31CPD ap + + - + + + + 7-30_3rd FCC_F2
9 22:09:23 lbp.200916.a400 11 C13CPD lbp + + - + + + + LBP-2-2 sref: reference peak not found default calibration done
18 21:58:28 ap.200916.a400 30 PROTON ap + + - + + + + 7-30_3rd FCC_F2
7 21:37:18 ap.200916.a400 21 P31CPD ap - + - - - + + 7-30_3rd FCC_F1
7 21:25:48 ap.200916.a400 20 PROTON ap + + - + + + + 7-30_3rd FCC_F1
11 20:00:02 cpo.200916.a400 15 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check - 10h sref: reference peak not found default calibration done
21 19:40:49 mci.200916.a400 10 PROTON mci + + - + + + + mci av90
17 19:10:30 av.200916.a400 10 PROTON av + + - - x + + 1-90 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
15 19:02:46 yd.200916.a400 30 PROTON yd + + - - + + + YD-500-205-crude sref: reference peak not found default calibration done
14 18:57:41 yd.200916.a400 20 PROTON yd + + - - x + + YD-507-203-fraction B topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
13 18:50:30 yd.200916.a400 10 PROTON yd + + - + + + + YD-507-203-fraction A
12 17:56:16 ap.200916.a400 11 P31CPD ap - + - - - + + 7-34
12 17:45:13 ap.200916.a400 10 PROTON ap + + - + + + + 7-34
24 16:55:08 cbc.200916.a400 11 COSY cbc - + - - - + + CBC143 crude
24 16:46:45 cbc.200916.a400 10 PROTON cbc + + - - + + + CBC143 crude
23 16:39:20 naa.200916.a400 10 PROTON naa + + - + + + + MEF103
16 16:21:12 cvh.200916.a400 30 PROTON cvh + + - + + + + CVI1-67 7-12 sref: reference peak not found default calibration done
11 16:00:02 cpo.200916.a400 14 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check - 6h sref: reference peak not found default calibration done
15 14:52:50 cvh.200916.a400 21 C13 cvh + + - + + + + CVI1-67 13-18 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
19 14:35:55 fr.200916.a400 11 COSY fr - + - - - + + FR-119-1E COSY
19 14:24:25 fr.200916.a400 10 PROTON fr + + - + + + + FR-119-1E -HNMR sref: reference peak not found default calibration done
15 14:16:45 cvh.200916.a400 20 PROTON cvh + + - + + + + CVI1-67 13-18
11 14:00:01 cpo.200916.a400 13 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check - 4h sref: reference peak not found default calibration done
12 13:53:22 pd.200916.a400 21 P31CPD pd - + - - - + + PD-259A_1
12 13:42:15 pd.200916.a400 20 PROTON pd + + - + + + + PD-259A_1
10 13:35:17 lbp.200916.a400 30 PROTON lbp + + - + + + + LBP-2-3 sref: reference peak not found default calibration done
14 13:10:28 cvh.200916.a400 10 PROTON cvh + + - + + + + CVI1-63
5 12:59:03 slb.200916.a400 51 F19CPD_KU slb - + - - - + +
5 12:51:52 slb.200916.a400 50 F19CPD_KU slb + + - - + + +
4 12:44:55 slb.200916.a400 40 PROTON slb + + - - + + + SLB_30.04.19_ax
3 12:37:51 slb.200916.a400 30 PROTON slb + + - - + + + SLB_32_ax
2 12:31:01 slb.200916.a400 20 PROTON slb + + - - + + + SLB_29_ax
1 12:23:18 slb.200916.a400 10 PROTON slb + + - + + + + SLB_29_eq
9 12:16:10 lbp.200916.a400 10 PROTON lbp + + - + + + + LBP-2-2 sref: reference peak not found default calibration done
11 12:00:02 cpo.200916.a400 12 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check - 2h sref: reference peak not found default calibration done
10 11:26:24 lbp.200916.a400 20 PROTON lbp + + - + + + + LBP-3-1-mix sref: reference peak not found default calibration done
11 11:00:01 cpo.200916.a400 11 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check - 1h sref: reference peak not found default calibration done
11 09:58:20 cpo.200916.a400 10 PROTON cpo + + - + + + + UB300 +5% Acetone - Stability check sref: reference peak not found default calibration done
22 09:20:11 pd.200916.a400 10 PROTON pd + + - + + + + PD-263-CR
22 03:24:30 rg.200915.a400 20 C13CPD rg + + - - + + + RGV_60 sref: reference peak not found default calibration done
17 02:33:47 mb.200915.a400 14 HMBC mb + + - + + + + THA1P1 HMBC
5 02:18:33 cyl.200915.a400 23 HSQCETGP cyl - + - - - + + MCD_CL-02-58
5 02:12:45 cyl.200915.a400 22 COSY cyl - + - - - + + MCD_CL-02-58
5 01:08:17 cyl.200915.a400 21 C13CPD cyl + + - - + + + MCD_CL-02-58 sref: reference peak not found default calibration done
7 23:04:43 bhgLV30_I.200915.a400 14 C13CPD bhg + + - + + + + sref: reference peak not found default calibration done
9 22:00:30 ap.200915.a400 33 C13CPD ap + + - + + + + 7-30_2nd FCC_F2 sref: reference peak not found default calibration done
9 21:36:44 ap.200915.a400 32 HSQC ap - + - - - + + 7-30_2nd FCC_F2
9 21:34:48 ap.200915.a400 31 P31CPD ap - + - - - + + 7-30_2nd FCC_F2
9 21:23:40 ap.200915.a400 30 PROTON ap + + - + + + + 7-30_2nd FCC_F2
23 19:26:28 aog_008_S.200915.a400 10 PROTON aog + + - - + + + sref: reference peak not found default calibration done
21 19:16:56 aog_008_P.200915.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
11 18:50:11 ap.200915.a400 21 P31CPD ap - + - - - + + 7-30_2nd FCC_F1
11 18:38:40 ap.200915.a400 20 PROTON ap + + - + + + + 7-30_2nd FCC_F1
16 17:40:52 cyl.200915.a400 30 PROTON cyl + + - + + + + MCD_CL-02-61 sref: reference peak not found default calibration done
20 16:10:00 fr.200915.a400 31 COSY fr - + - - - + + FR-120-1B - COSY
20 15:59:25 fr.200915.a400 30 PROTON fr + + - + + + + FR-120-1B - HNMR sref: reference peak not found default calibration done
4 15:14:48 krb.200915.a400 30 PROTON krb + + - - + + +
2 15:06:10 pd.200915.a400 10 PROTON pd + + - - + + + PD-253A sref: reference peak not found default calibration done
22 14:50:27 rg.200915.a400 11 C13 rg - + - - - + + RGV_60 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
22 14:43:28 rg.200915.a400 10 PROTON rg + + - + + + + RGV_60
17 14:21:47 mb.200915.a400 13 HSQC mb + + - - + + + THA1P1 HSQC
20 14:15:51 ms.200915.a400 11 COSY ms - + - - - + + POTz crude
20 14:08:44 ms.200915.a400 10 PROTON ms + + - - + + + POTz crude
13 13:51:21 krb.200915.a400 20 PROTON krb + + - - + + + KB1-8_F1
17 13:45:26 mb.200915.a400 12 COSY mb - + - - - + + THA1P1 COSY
17 13:29:39 mb.200915.a400 11 C13 mb - + - - - + + THA1P1 13C au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
17 13:22:11 mb.200915.a400 10 PROTON mb + + - + + + + THA1P1 1H
10 12:50:41 gg.200915.a400 10 PROTON gg + + - + + + + GG01-100_1
5 12:27:29 cyl.200915.a400 20 PROTON cyl + + - + + + + MCD_CL-02-58 sref: reference peak not found default calibration done
3 12:11:06 krb.200915.a400 10 PROTON krb + + - + + + +
7 11:49:31 bhgLV30_I.200915.a400 13 TOCSY bhg - + - - - + +
7 11:34:02 bhgLV30_I.200915.a400 12 HSQC bhg - + - - - + +
7 11:28:18 bhgLV30_I.200915.a400 11 COSY bhg - + - - - + +
7 11:12:06 bhgLV30_I.200915.a400 10 PROTON bhg + + - + + + +
24 10:51:27 mmsh.200915.a400 20 PROTON mmsh + + - + + + + MH01-PEG-METHYL-CL
2 10:44:38 cyl.200915.a400 10 PROTON cyl + + - + + + + CL-02-58 sref: reference peak not found default calibration done
15 10:35:28 yst.200915.a400 10 PROTON yst + + - + + + + VF-15
19 10:29:37 fr.200915.a400 21 COSY fr - + - - - + + FR-119-1B - COSY2
19 10:21:07 fr.200915.a400 20 PROTON fr + + - - + + + FR-119-1B - HNMR2
12 10:11:45 mmsh.200915.a400 10 PROTON mmsh + + - - x + + MH01-BASE1-5-5-N-OXIDE-T4-STEP3 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
8 09:36:36 cvh.200915.a400 11 C13 cvh + + - - + + + CVI1-66 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
19 09:30:48 fr.200915.a400 11 COSY fr - + - - - + + FR-119-1B - COSY
19 09:21:26 fr.200915.a400 10 PROTON fr + + - - x + + FR-119-1B - HNMR topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
8 09:13:55 cvh.200915.a400 10 PROTON cvh + + - + + + + CVI1-66
14 08:45:29 ap.200915.a400 10 PROTON ap + + - + + + + 7-31_2nd FCC_F1
1 07:48:05 ki514_1.200915.a400 10 PROTON ki + + - + + + + KI 514-1 sref: reference peak not found default calibration done
18 22:46:18 ap.200914.a400 81 P31CPD ap - + - - - + + 7-31_2nd FCC_F3 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200914.a400/81/pdata/1/peaks!
18 22:34:48 ap.200914.a400 80 PROTON ap + + - - + + + 7-31_2nd FCC_F3
17 22:27:50 ap.200914.a400 71 P31CPD ap + + - - + + + 7-31_2nd FCC_F2
16 22:07:06 ap.200914.a400 62 HSQC ap + + - - + + + 7-31_2nd FCC_F1
17 21:55:38 ap.200914.a400 70 PROTON ap + + - - + + + 7-31_2nd FCC_F2
16 21:53:27 ap.200914.a400 61 P31CPD ap - + - - - + + 7-31_2nd FCC_F1
16 21:42:03 ap.200914.a400 60 PROTON ap + + - + + + + 7-31_2nd FCC_F1
9 20:23:21 jiz.200914.a400 30 PROTON jiz + + - - + + + JZ08_120 sref: reference peak not found default calibration done
8 20:07:09 jiz.200914.a400 20 PROTON jiz + + - - + + + Tertbutyl amine sref: reference peak not found default calibration done
7 19:50:30 jiz.200914.a400 10 PROTON jiz + + - + + + + Ts2O sref: reference peak not found default calibration done
18 19:48:33 ap.200914.a400 51 P31CPD ap - + - - - + + 7-30_F4
18 19:37:46 ap.200914.a400 50 PROTON ap + + - - + + + 7-30_F4
17 19:35:33 ap.200914.a400 41 P31CPD ap - + - - - + + 7-30_F3
17 19:23:50 ap.200914.a400 40 PROTON ap + + - + + + + 7-30_F3
22 18:35:39 yst273.200914.a400 11 HSQC yst - + - - - + +
22 18:27:58 yst273.200914.a400 10 PROTON yst + + - + + + +
15 18:09:21 lss.200914.a400 20 PROTON lss + + - - x + + LSS-15_9-10 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
2 18:02:09 yd.200914.a400 20 PROTON yd + + - + + + + YD-600-200-zir safi-washed with acetone sref: reference peak not found default calibration done
1 17:55:15 yd.200914.a400 10 PROTON yd + + - + + + + YD-600-200-white solid-washed with acetone sref: reference peak not found default calibration done
24 17:53:19 ap.200914.a400 31 P31CPD ap - + - - - + + 7-30_F2
24 17:42:50 ap.200914.a400 30 PROTON ap + + - - + + + 7-30_F2
23 17:40:45 ap.200914.a400 21 P31CPD ap - + - - - + + 7-30_F1
23 17:29:01 ap.200914.a400 20 PROTON ap + + - + + + + 7-30_F1
13 17:21:55 cyl.200914.a400 10 PROTON cyl + + - + + + + cl-black
6 17:14:19 aln.200914.a400 10 PROTON aln + + - - + + + DTT_Check sref: reference peak not found default calibration done
17 17:08:06 ye_27M_F2r.200914.a400 10 F19CPD_KU ye + + - - + + +
16 17:01:41 ye_27M_Fr.200914.a400 10 F19CPD_KU ye + + - - + + +
2 16:41:59 mmsh.200914.a400 20 PROTON mmsh + + - + + + + mh01-base1-5-5-t4-step4-2 sref: reference peak not found default calibration done
22 16:11:59 yst.200914.a400 11 C13 yst - + - - - + + YST-273 5h au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
22 16:04:22 yst.200914.a400 10 PROTON yst + + - + + + + YST-273 5h
14 15:48:24 ed.200914.a400 11 C13 ed - + - - - + + thiophen pinacole, fraction 4 au_zg_max30min: --- au_zg_max30min finished ---
14 15:40:26 ed.200914.a400 10 PROTON ed + + - + + + + thiophen pinacole, fraction 4
17 15:34:18 ye_27M_F2r.200914.a400 10 F19CPD_KU ye + + - - + + +
16 15:28:17 ye_27M_Fr.200914.a400 10 F19CPD_KU ye + + - - + + +
15 15:21:47 ye_26M_Fr.200914.a400 10 F19CPD_KU ye + + - + + + +
10 15:02:56 mmsh.200914.a400 10 PROTON mmsh + + - + + + + mh01-base1-5-5-t4
7 14:23:20 ye_26M_Fc.200914.a400 10 F19CPD_KU ye + + - - + + +
9 14:17:16 ye_27M_F2c.200914.a400 10 F19CPD_KU ye + + - - + + +
8 14:10:26 ye_27M_Fc.200914.a400 10 F19CPD_KU ye + + - + + + +
7 14:04:06 ye_26M_Fc.200914.a400 10 F19CPD_KU ye + + - + + + +
4 13:46:56 om_i_40.200914.a400 10 Quant_KU om + + - - + + + pulsecal: setting option 'sn' for organic solvent (DMSO), sref: reference peak not found default calibration done
3 13:37:28 aog_004_4.200914.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
18 12:12:58 rr.200914.a400 140 PROTON rr + + - - + + + 168 pink-yellow gradient (mixed it)
17 12:06:44 rr.200914.a400 130 PROTON rr + + - - + + + 168 brown
16 12:00:23 rr.200914.a400 120 PROTON rr + + - - + + + 166
15 11:54:15 rr.200914.a400 110 PROTON rr + + - - + + + 164
14 11:48:05 rr.200914.a400 100 PROTON rr + + - - + + + 161
13 11:40:44 rr.200914.a400 90 PROTON rr + + - + + + + 160
21 11:32:30 lss.200914.a400 10 PROTON lss + + - - + + + LSS-16 pure
20 11:21:25 gg.200914.a400 10 PROTON gg + + - - + + + GG01-92_1_after purification
19 11:05:23 civ.200914.a400 11 C13 civ - + - - - + + CIV1-10 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
19 10:57:17 civ.200914.a400 10 PROTON civ + + - + + + + CIV1-10
12 10:51:16 rr.200914.a400 80 PROTON rr + + - - + + + 159
11 10:44:50 rr.200914.a400 70 PROTON rr + + - - + + + 158
10 10:38:16 rr.200914.a400 60 PROTON rr + + - + + + + 157
9 10:02:08 rr.200914.a400 50 PROTON rr + + - - + + + 156
8 09:56:07 rr.200914.a400 40 PROTON rr + + - - + + + 155
7 09:49:42 rr.200914.a400 30 PROTON rr + + - - + + + 154
6 09:43:17 rr.200914.a400 20 PROTON rr + + - - + + + 142
5 09:35:46 rr.200914.a400 10 PROTON rr + + - + + + + Ref. 25 mM
12 09:23:52 fr.200914.a400 10 PROTON fr + + - + + + + FR-119-1A - HNMR
3 09:21:34 pd.200914.a400 11 P31CPD pd - + - - - + + PD3-259C
3 09:15:04 pd.200914.a400 10 PROTON pd + + - + + + + PD3-259C
3 09:07:20 ap.200914.a400 10 PROTON ap + + - + + + + PD-259C
16 14:57:47 ap.200913.a400 30 PROTON ap + + - + + + + 7-33_crude
2 14:51:27 msPyPyTz.200913.a400 10 PROTON ms + + - - + + + Py2Tz DMSO sref: reference peak not found default calibration done
1 14:49:19 ms.200913.a400 11 F19CPD_KU ms - + - - - + + N2 Fluor. Py2Tz crude
1 14:42:48 ms.200913.a400 10 PROTON ms + + - + + + + N2 Fluor. Py2Tz crude
13 13:49:54 ap.200913.a400 22 F19CPD_KU ap - + - - - + + 7-33_crude
13 13:47:48 ap.200913.a400 21 P31CPD ap - + - - - + + 7-33_crude
13 13:36:41 ap.200913.a400 20 PROTON ap + + - + + + + 7-33_crude
16 13:23:01 ap.200913.a400 12 F19CPD_KU ap - + - - - + + 7-32_crude
16 13:20:58 ap.200913.a400 11 P31CPD ap - + - - - + + 7-32_crude
16 13:10:09 ap.200913.a400 10 PROTON ap + + - + + + + 7-32_crude
11 03:40:51 ap.200912.a400 51 P31CPD ap - + - - - + + 7-31_F3
11 03:27:47 ap.200912.a400 50 PROTON ap + + - - + + + 7-31_F3
16 03:25:25 ap.200912.a400 44 F19CPD_KU ap - + - - - + + 7-31_F2
16 03:23:06 ap.200912.a400 43 PROTON ap - + - - - + + 7-31_F2
16 03:20:44 ap.200912.a400 41 P31CPD ap - + - - - + + 7-31_F2
16 03:07:14 ap.200912.a400 40 PROTON ap + + - + + + + 7-31_F2
10 02:02:28 jmr.200912.a400 11 C13CPD jmr + + - + + + + sref: reference peak not found default calibration done
12 01:47:03 yst.200912.a400 12 HSQC yst - + - - - + + YST-272-1
12 23:42:48 yst.200912.a400 11 C13CPD yst + + - + + + + YST-272-1 sref: reference peak not found default calibration done
16 23:22:10 ap.200912.a400 42 HSQC ap + + - - + + + 7-31_F2
7 22:22:19 ap.200912.a400 34 C13CPD ap - + - - - + + 7-31_F1 sref: reference peak not found default calibration done
7 22:06:38 ap.200912.a400 33 HSQC ap - + - - - + + 7-31_F1
7 22:04:36 ap.200912.a400 31 P31CPD ap - + - - - + + 7-31_F1
7 21:52:43 ap.200912.a400 30 PROTON ap + + - + + + + 7-31_F1
10 17:48:10 jmr.200912.a400 10 PROTON jmr + + - + + + + sref: reference peak not found default calibration done
17 15:12:53 ms093cr.200912.a400 10 PROTON ms + + - + + + + MS1060-093 crude
13 14:11:13 ap.200912.a400 21 P31CPD ap - + - - - + + 7-25_Rev C18_40mg_f7,8
13 14:00:13 ap.200912.a400 20 PROTON ap + + - - + + + 7-25_Rev C18_40mg_f7,8
16 13:57:46 ap.200912.a400 11 P31CPD ap - + - - - + + 7-25_Rev C18_40mg_f6
16 13:47:00 ap.200912.a400 10 PROTON ap + + - + + + + 7-25_Rev C18_40mg_f6
12 12:23:38 yst.200912.a400 10 PROTON yst + + - + + + + YST-272-1
8 10:30:05 ms092.200912.a400 11 C13 ms - + - - - + + MS1059-092 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 10:23:11 ms092.200912.a400 10 PROTON ms + + - + + + + MS1059-092
6 01:14:08 lbp.200911.a400 20 C13CPD lbp + + - + + + + LBP-2-1-Carbon sref: reference peak not found default calibration done
13 00:07:57 av.200911.a400 21 C13CPD av + + - + + + + 1-89 2nd sref: reference peak not found default calibration done
10 23:04:30 jmr.200911.a400 11 C13CPD jmr + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
11 22:00:10 jmr.200911.a400 21 C13CPD jmr + + - + + + + sref: reference peak not found default calibration done
5 20:14:14 gb.200911.a400 50 PROTON gb + + - + + + + GB-18-1-CRUDE
15 19:54:41 pd.200911.a400 21 P31CPD pd - + - - - + + PD3-259-F4
15 19:47:58 pd.200911.a400 20 PROTON pd + + - - + + + PD3-259-F4
14 19:46:00 pd.200911.a400 11 P31CPD pd - + - - - + + PD3-259-F3
14 19:39:20 pd.200911.a400 10 PROTON pd + + - + + + + PD3-259-F3
9 19:23:30 gg.200911.a400 10 PROTON gg + + - + + + + GG01-100_Solid sref: reference peak not found default calibration done
22 19:16:42 yd.200911.a400 60 PROTON yd + + - - + + + YD-506-201-yellow oil sref: reference peak not found default calibration done
21 19:09:43 yd.200911.a400 50 PROTON yd + + - - + + + YD-600-200-crude
20 19:02:29 yd.200911.a400 40 PROTON yd + + - + + + + YD-600-199-crude
7 18:40:02 mciMBexF34.200911.a400 10 PROTON mci + + - + + + +
13 17:29:42 av.200911.a400 20 PROTON av + + - + + + + 1-89 2nd
13 17:13:54 av.200911.a400 10 PROTON av + + - - x + + 1-89 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
3 17:05:50 par.200911.a400 20 PROTON par + + - + + + + reagent-tertbutylamunbromi
12 17:03:41 ap.200911.a400 21 P31CPD ap - + - - - + + 7-26_2nd FCC_F0
12 16:51:55 ap.200911.a400 20 PROTON ap + + - + + + + 7-26_2nd FCC_F0
19 16:44:14 yd.200911.a400 30 PROTON yd + + - + + + + YD-506-201-C-yellow oil sref: reference peak not found default calibration done
18 16:37:37 yd.200911.a400 20 PROTON yd + + - + + + + YD-506-201-B-white solid sref: reference peak not found default calibration done
17 16:30:47 yd.200911.a400 10 PROTON yd + + - + + + + YD-506-201-pure-A sref: reference peak not found default calibration done
6 16:16:24 lbp.200911.a400 10 PROTON lbp + + - + + + + LBP-2-1 sref: reference peak not found default calibration done
2 14:26:45 mef.200911.a400 11 C13 mef - + - - - + + MEF101_extr. au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 14:19:40 mef.200911.a400 10 PROTON mef + + - + + + + MEF101_extr. sref: reference peak not found default calibration done
24 14:12:15 gb.200911.a400 40 PROTON gb + + - - + + + GB-17-1-AFTERPURIFICATION sref: reference peak not found default calibration done
23 14:04:33 gb.200911.a400 30 PROTON gb + + - + + + + FILTRATO
3 13:27:36 par.200911.a400 10 PROTON par + + - + + + + 105-002-C
14 12:33:04 fr.200911.a400 11 COSY fr - + - - - + + FR-118-1B - COSY
14 12:22:10 fr.200911.a400 10 PROTON fr + + - + + + + FR-118-1B - HNMR sref: reference peak not found default calibration done
8 12:06:22 mci2ex4f30.200911.a400 12 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 12:00:31 mci2ex4f30.200911.a400 11 COSY mci - + - - - + +
8 11:54:01 mci2ex4f30.200911.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
5 11:37:29 gb.200911.a400 20 PROTON gb + + - - x + + gb-17-1-puremaybe topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
4 11:29:53 gb.200911.a400 10 PROTON gb + + - + + + + GB-17-1-CRUDEAGAIN sref: reference peak not found default calibration done
10 10:45:33 jmr.200911.a400 10 PROTON jmr + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
11 10:39:04 jmr.200911.a400 20 PROTON jmr + + - + + + + sref: reference peak not found default calibration done
7 10:20:48 ap.200911.a400 11 P31CPD ap - + - - - + + 7-29_crude
7 10:09:46 ap.200911.a400 10 PROTON ap + + - + + + + 7-29_crude
20 09:41:02 umb.200911.a400 10 F19CPD_KU umb + + - + + + +
14 05:55:06 ap.200910.a400 41 P31CPD ap - + - - - + + 7-26_2nd FCC_F3
14 05:44:25 ap.200910.a400 40 PROTON ap + + - - + + + 7-26_2nd FCC_F3
13 05:42:31 ap.200910.a400 31 P31CPD ap - + - - - + + 7-26_2nd FCC_F2
13 05:32:01 ap.200910.a400 30 PROTON ap + + - - + + + 7-26_2nd FCC_F2
12 05:29:48 ap.200910.a400 21 P31CPD ap - + - - - + + 7-26_2nd FCC_F1
12 05:18:10 ap.200910.a400 20 PROTON ap + + - + + + + 7-26_2nd FCC_F1
9 04:10:44 lbp.200910.a400 30 C13CPD lbp + + - + + + + LBP-1-3_HRCarbon sref: reference peak not found default calibration done
17 03:05:43 ms092w.200910.a400 11 C13CPD ms + + - - + + + MS1059-092 wash sref: reference peak not found default calibration done
11 23:05:10 cpo629.200910.a400 12 C13CPD cpo + + - - + + + CPO629-211 Fr 6-7 sref: reference peak not found default calibration done
8 22:00:05 av.200910.a400 21 C13CPD av + + - + + + + 1-87 2 FCC 21-26 sref: reference peak not found default calibration done
8 18:25:12 av.200910.a400 20 PROTON av + + - + + + + 1-87 2 FCC 21-26 sref: reference peak not found default calibration done
4 18:15:26 aog_005.200910.a400 10 PROTON aog + + - + + + +
22 18:08:23 gb.200910.a400 50 PROTON gb + + - - + + + GB-17-1-4
21 18:00:21 gb.200910.a400 40 PROTON gb + + - + + + + GB-17-1-3 sref: reference peak not found default calibration done
8 17:51:28 mci2ex4f3234.200910.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
6 17:44:33 mci2ex4f30.200910.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
5 17:37:16 kd.200910.a400 10 PROTON kd + + - - + + + crude 3
23 17:35:17 ap.200910.a400 11 P31CPD ap - + - - - + + 7-30_1st step
23 17:23:31 ap.200910.a400 10 PROTON ap + + - - + + + 7-30_1st step
3 17:18:25 gb.200910.a400 30 PROTON gb + + - - x + + GB-17-1-3 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
2 17:11:25 gb.200910.a400 20 PROTON gb + + - - + + + gb-17-1-2 sref: reference peak not found default calibration done
1 17:04:31 gb.200910.a400 10 PROTON gb + + - + + + + GB-17-1-1 sref: reference peak not found default calibration done
16 16:25:10 ial_23_2.200910.a400 10 PROTON ial + + - + + + +
14 16:07:06 jn239mixx2.200910.a400 10 PROTON jn + + - + + + + jn239 240 241 mix x2 sref: reference peak not found default calibration done
10 15:18:32 lbp.200910.a400 20 PROTON lbp + + - - + + + LBP-1-4 sref: reference peak not found default calibration done
9 15:10:58 lbp.200910.a400 10 PROTON lbp + + - + + + + LBP-1-3 sref: reference peak not found default calibration done
17 15:03:27 ms092w.200910.a400 10 PROTON ms + + - + + + + MS1059-092 wash sref: reference peak not found default calibration done
15 12:49:34 gg.200910.a400 20 PROTON gg + + - + + + + GG01-94_Product_3rd
20 12:06:47 cc.200910.a400 12 P31CPD cc + + - + + + + Mingshi Remdesivir,072020
17 11:58:37 av.200910.a400 10 PROTON av + + - + + + + 1-87 combined
20 11:31:15 cc.200910.a400 11 P31 cc + + - + + + + Mingshi Remdesivir,072020
18 11:20:21 fr.200910.a400 20 PROTON fr + + - - + + + FR-118-1A - HNMR
12 11:03:55 gg.200910.a400 10 PROTON gg + + - - + + + GG01-94_Product_Again
7 10:56:29 ms092c.200910.a400 10 PROTON ms + + - + + + + MS1059-092 sref: reference peak not found default calibration done
20 10:50:20 cc.200910.a400 10 PROTON cc + + - + + + + Mingshi Remdesivir,072020 sref: reference peak not found default calibration done
18 10:49:08 fr.200910.a400 10 PROTON fr x - - - - - - FR-118-1A - HNMR Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 18
13 10:41:43 cbc.200910.a400 10 PROTON cbc + + - - + + + SM check
11 10:11:40 cpo629.200910.a400 11 C13 cpo - + - - - + + CPO629-211 Fr 6-7 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 09:59:30 cpo629.200910.a400 10 PROTON cpo + + - + + + + CPO629-211 Fr 6-7
15 23:04:02 av.200909.a400 31 C13CPD av + + - - + + + 1-88 sref: reference peak not found default calibration done
13 22:00:11 av.200909.a400 11 C13APT_KU_night av + + - + + + + 1-84 sref: reference peak not found default calibration done
24 20:33:57 gg.200909.a400 50 PROTON gg + + - + + + + GG01-98 sref: reference peak not found default calibration done
23 20:22:25 gg.200909.a400 40 PROTON gg + + - + + + + GG01-94_Product
19 20:14:52 mci2ex4f5.200909.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
18 20:08:00 mci2ex4f2.200909.a400 10 PROTON mci + + - + + + +
15 18:22:12 av.200909.a400 30 PROTON av + + - - + + + 1-88 sref: reference peak not found default calibration done
14 18:17:19 av.200909.a400 20 PROTON av + + - - x + + 1-87 10 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
13 18:10:23 av.200909.a400 10 PROTON av + + - + + + + 1-84 sref: reference peak not found default calibration done
12 17:53:30 gg.200909.a400 30 PROTON gg + + - - + + + GG01-94_Starting_Material
11 17:45:10 gg.200909.a400 20 PROTON gg + + - + + + + GG01-94_Org
5 17:32:50 aog_004_3.200909.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
16 15:37:28 em1040.200909.a400 10 PROTON emr + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
15 15:29:07 ial_41_1.200909.a400 10 PROTON ial + + - + + + +
11 14:18:50 cvh.200909.a400 20 PROTON cvh + + - + + + + CVI1-60
1 14:04:39 aog_004_2.200909.a400 10 PROTON aog + + - + + + + sref: reference peak not found default calibration done
10 13:53:31 ms092cr.200909.a400 11 COSY ms - + - - - + + MS1059-092 crude
10 13:45:33 ms092cr.200909.a400 10 PROTON ms + + - + + + + MS1059-092 crude sref: reference peak not found default calibration done
7 13:34:52 par.200909.a400 10 PROTON par + + - + + + + 105-001-CC
10 11:28:05 cvh.200909.a400 10 PROTON cvh + + - + + + + CVI1-59
20 10:55:23 jj.200909.a400 20 PROTON jj + + - - + + + JJ33 1H_3
6 10:46:52 fr.200909.a400 10 PROTON fr + + - + + + + FR-103-2A - HNMR
1 10:18:36 aog.200909.a400 11 C13APT_KU aog + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 09:15:33 gg.200909.a400 10 PROTON gg + + - + + + + GG01-92_Product_2 sref: reference peak not found default calibration done
24 08:43:58 jj.200909.a400 10 PROTON jj + + - + + + + 1H Cloroform sref: reference peak not found default calibration done
8 23:04:34 emr.200908.a400 11 C13CPD emr + + - - + + + 5-china sample sref: reference peak not found default calibration done
11 22:00:06 ays.200908.a400 10 C13CPD ays + + - + + + + FmocHN-Gly-Glyco-OtBu 13C sref: reference peak not found default calibration done
9 17:19:20 pd.200908.a400 10 PROTON pd + + - + + + + PD3-254CR sref: reference peak not found default calibration done
8 17:10:32 emr.200908.a400 10 PROTON emr + + - + + + + 5-china sample sref: reference peak not found default calibration done
4 14:02:14 umb.200908.a400 10 PROTON umb x - - - - - - JS-156 Sample Changer Fatal Error: Error: Error: STOP_CHANGER 1000 STOP_CHANGER SampleTransporter: LoadSample failed, sample no longer detected by upper light bar
20 13:44:18 fr.200908.a400 10 PROTON fr + + - + + + + FR-102-2B - HNMR
4 13:41:52 umbjos503.200908.a400 11 F19CPD_KU umb - + - - - + +
4 13:34:57 umbjos503.200908.a400 10 PROTON umb + + - + + + + sref: reference peak not found default calibration done
17 13:30:00 em1030iso2.200908.a400 10 PROTON emr + + - - x + + em isomer 2 (1030) topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
16 13:23:02 em1030iso1.200908.a400 10 PROTON emr + + - - + + + em isomer 1 (1030) sref: reference peak not found default calibration done
15 13:16:40 jniso2.200908.a400 10 PROTON emr + + - - + + + jn isomer 2
14 13:10:22 jniso1.200908.a400 10 PROTON emr + + - - + + + jn isomer 1
10 13:03:09 ed.200908.a400 10 PROTON ed + + - + + + + furan carboxylsyre m. cyanophenyl, test
8 12:49:11 yst.200908.a400 20 PROTON yst + + - - + + + YST-272 crude
7 12:40:38 yst.200908.a400 10 PROTON yst + + - + + + + VF-35
13 12:12:39 av.200908.a400 10 PROTON av + + - - + + + 4brbuty
11 11:11:36 ap.200908.a400 13 HSQC ap x - - - - - - 7-27_F5 Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 11
19 11:04:22 lss.200908.a400 10 PROTON lss + + - - + + + LSS-FC2-p
9 10:48:36 mci2ex3.200908.a400 11 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
9 10:40:44 mci2ex3.200908.a400 10 PROTON mci + + - - + + +
22 10:33:33 ms.200908.a400 10 PROTON ms + + - - + + + BODTz crude TEOF tr
14 10:21:52 gg.200908.a400 10 PROTON gg + + - + + + + GG01-92
11 10:05:49 ap.200908.a400 14 C13 ap - + - - - + + 7-27_F5 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 10:03:25 ap.200908.a400 12 F19CPD_KU ap - + - - - + + 7-27_F5
11 10:01:11 ap.200908.a400 11 P31CPD ap - + - - - + + 7-27_F5
11 09:50:07 ap.200908.a400 10 PROTON ap + + - + + + + 7-27_F5 sref: reference peak not found default calibration done
6 09:31:02 cvh.200908.a400 10 PROTON cvh + + - + + + + CVI1-60
13 00:45:11 av.200907.a400 11 C13CPD av + + - - + + + AV1-85 11 17 sref: reference peak not found default calibration done
17 23:40:09 ial_40_1.200907.a400 11 C13CPD ial + + - + + + + sref: reference peak not found default calibration done
16 22:35:38 yst.200907.a400 20 C13CPD yst + + - + + + + LBP-1-1 sref: reference peak not found default calibration done
1 22:00:21 jop.200907.a400 12 C13 jop + + - + + + + JOP_V_214_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
20 19:06:25 ap.200907.a400 73 HSQC ap - + - - - + + 6-27_F4
20 19:04:10 ap.200907.a400 72 F19CPD_KU ap - + - - - + + 6-27_F4
20 19:02:14 ap.200907.a400 71 P31CPD ap - + - - - + + 6-27_F4 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200907.a400/71/pdata/1/peaks!
20 18:51:32 ap.200907.a400 70 PROTON ap + + - + + + + 6-27_F4
17 18:32:21 ial_40_1.200907.a400 10 PROTON ial + + - - + + +
13 18:25:21 av.200907.a400 10 PROTON av + + - + + + + AV1-85 11 17 sref: reference peak not found default calibration done
4 17:46:34 yst.200907.a400 30 PROTON yst + + - + + + + YST-257-3
24 17:44:40 ap.200907.a400 61 P31CPD ap - + - - - + + 7-28_F1 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200907.a400/61/pdata/1/peaks!
24 17:33:56 ap.200907.a400 60 PROTON ap + + - - + + + 7-28_F1
23 17:32:02 ap.200907.a400 51 P31CPD ap - + - - - + + 7-28_F5 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200907.a400/51/pdata/1/peaks!
23 17:21:30 ap.200907.a400 50 PROTON ap + + - + + + + 7-28_F5
19 17:03:14 lss.200907.a400 10 PROTON lss + + - + + + + LSS-15 confirmed sref: reference peak not found default calibration done
22 17:01:20 ap.200907.a400 41 P31CPD ap - + - - - + + 7-28_F2 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200907.a400/41/pdata/1/peaks!
22 16:50:35 ap.200907.a400 40 PROTON ap + + - - + + + 7-28_F2 sref: reference peak not found default calibration done
21 16:48:40 ap.200907.a400 31 P31CPD ap - + - - - + + 7-28_F3 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200907.a400/31/pdata/1/peaks!
21 16:37:23 ap.200907.a400 30 PROTON ap + + - + + + + 7-28_F3
18 16:29:36 gg.200907.a400 20 PROTON gg + + - + + + + GG01-90_Product sref: reference peak not found default calibration done
15 16:06:37 yst.200907.a400 10 PROTON yst + + - + + + + LBP-1-2 sref: reference peak not found default calibration done
20 16:03:44 ap.200907.a400 21 P31CPD ap - + - - - + + 7-28_F4 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200907.a400/21/pdata/1/peaks!
20 15:52:55 ap.200907.a400 20 PROTON ap + + - + + + + 7-28_F4
9 15:08:27 cvh.200907.a400 30 PROTON cvh + + - + + + + CVI1-39
1 14:47:27 jop.200907.a400 11 C13 jop - + - - - + + JOP_V_214_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 14:40:06 jop.200907.a400 10 PROTON jop + + - - + + + JOP_V_214_1 sref: reference peak not found default calibration done
7 14:32:03 cvh.200907.a400 20 PROTON cvh + + - + + + + CVI1-60 15-22 sref: reference peak not found default calibration done
10 14:20:30 mci2ex3.200907.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
8 13:33:50 cvh.200907.a400 10 PROTON cvh + + - + + + + CVI1-59
18 12:48:43 fr.200907.a400 10 PROTON fr + + - + + + + FR-116-1C - HNMR IN DMSO sref: reference peak not found default calibration done
13 12:19:48 ms.200907.a400 20 PROTON ms + + - - + + + 6-CN nicAc sref: reference peak not found default calibration done
12 12:13:04 ms.200907.a400 10 PROTON ms + + - + + + + 6-CN nicAcCl sref: reference peak not found default calibration done
10 09:57:00 ays.200907.a400 10 PROTON ays + + - + + + + FmocHN-Gly-O-Glycolicacid-tBu sref: reference peak not found default calibration done
7 09:54:41 ap.200907.a400 12 F19CPD_KU ap - + - - - + + 7-28_crude
7 09:52:45 ap.200907.a400 11 P31CPD ap - + - - - + + 7-28_crude
7 09:42:19 ap.200907.a400 10 PROTON ap + + - + + + + 7-28_crude
24 08:59:38 gg.200907.a400 11 COSY gg - + - - - + + GG01-90_Byproduct
24 08:51:47 gg.200907.a400 10 PROTON gg + + - + + + + GG01-90_Byproduct sref: reference peak not found default calibration done
21 22:13:48 at1076_8.200906.a400 10 PROTON at + + - - + + +
22 22:02:35 at107st.200906.a400 10 PROTON at + + - - + + +
11 21:55:17 atsf.200906.a400 10 PROTON at + + - + + + +
15 12:47:42 ap.200906.a400 41 P31CPD ap - + - - - + + 7-24_F1 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200906.a400/41/pdata/1/peaks!
15 12:37:17 ap.200906.a400 40 PROTON ap + + - - + + + 7-24_F1 sref: reference peak not found default calibration done
14 12:35:14 ap.200906.a400 31 P31CPD ap - + - - - + + 7-24_F4
14 12:19:15 ap.200906.a400 30 PROTON ap + + - + + + + 7-24_F4 sref: reference peak not found default calibration done
6 11:52:45 ap.200906.a400 22 F19CPD_KU ap - + - - - + + 7-24_F5
6 11:50:41 ap.200906.a400 21 P31CPD ap - + - - - + + 7-24_F5
6 11:34:16 ap.200906.a400 20 PROTON ap + + - + + + + 7-24_F5 sref: reference peak not found default calibration done
7 11:24:07 ap.200906.a400 12 F19CPD_KU ap - + - - - + + 7-27_crude
7 11:21:52 ap.200906.a400 11 P31CPD ap - + - - - + + 7-27_crude
7 11:11:06 ap.200906.a400 10 PROTON ap + + - + + + + 7-27_crude
19 22:00:11 atcom.200905.a400 10 C13CPD at + + - + + + + sref: reference peak not found default calibration done
22 18:44:32 ap.200905.a400 21 P31CPD ap - + - - - + + 7-26_F6
22 18:33:24 ap.200905.a400 20 PROTON ap + + - + + + + 7-26_F6
10 16:29:05 cyl.200905.a400 10 PROTON cyl + + - + + + + MCD_CL-02-52 sref: reference peak not found default calibration done
21 15:49:57 ap.200905.a400 11 P31CPD ap - + - - - + + 7-25_crude
21 15:39:16 ap.200905.a400 10 PROTON ap + + - + + + + 7-25_crude
15 03:49:25 ap.200904.a400 61 P31CPD ap - + - - - + + 7-26_F5
15 03:38:12 ap.200904.a400 60 PROTON ap + + - - + + + 7-26_F5
14 02:38:30 ap.200904.a400 54 C13CPD ap - + - - - + + 7-26_F4 sref: reference peak not found default calibration done
14 02:32:41 ap.200904.a400 53 COSY ap - + - - - + + 7-26_F4
14 02:17:01 ap.200904.a400 52 HSQC ap - + - - - + + 7-26_F4
14 02:15:05 ap.200904.a400 51 P31CPD ap - + - - - + + 7-26_F4
14 02:07:02 ap.200904.a400 50 PROTON ap + + - - + + + 7-26_F4
10 02:05:07 ap.200904.a400 41 P31CPD ap - + - - - + + 7-26_F1
10 01:53:58 ap.200904.a400 40 PROTON ap + + - - + + + 7-26_F1
12 01:51:51 ap.200904.a400 21 P31CPD ap - + - - - + + 7-26_F3
12 01:40:49 ap.200904.a400 20 PROTON ap + + - + + + + 7-26_F3
3 00:51:01 gb.200904.a400 21 ROESY gb + + - - x + + gb-16-1-crude topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
6 00:00:08 jop.200904.a400 24 ROESY jop + + - + + + + JOP_V_207_1_T11
24 22:55:27 ki407_6.200904.a400 11 C13CPD ki + + - + + + + KI 407-6 sref: reference peak not found default calibration done
23 22:04:21 gb.200904.a400 11 ROESY gb + + - + + + + GB-15-1
11 22:02:14 ap.200904.a400 11 P31CPD ap - + - - - + + 7-26_F2
11 21:52:03 ap.200904.a400 10 PROTON ap + + - - + + + 7-26_F2
10 21:40:37 ap.200904.a400 30 PROTON ap + + - + + + + 7-25_F1
18 21:33:38 atorange2.200904.a400 10 PROTON at + + - - + + +
17 21:26:05 atorange.200904.a400 10 PROTON at + + - + + + +
19 19:13:55 atcon.200904.a400 10 PROTON at + + - + + + +
3 18:45:10 gb.200904.a400 20 PROTON gb + + - + + + + gb-16-1-crude
20 18:35:59 at42_46.200904.a400 10 PROTON at + + - + + + +
6 17:14:00 jop.200904.a400 23 HSQC jop - + - - - + + JOP_V_207_1_T11
6 17:08:10 jop.200904.a400 22 COSY jop - + - - - + + JOP_V_207_1_T11
6 16:52:02 jop.200904.a400 21 C13 jop - + - - - + + JOP_V_207_1_T11 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
6 16:45:02 jop.200904.a400 20 PROTON jop + + - + + + + JOP_V_207_1_T11 sref: reference peak not found default calibration done
7 16:25:54 lss.200904.a400 20 PROTON lss + + - + + + + LSS-15 sref: reference peak not found default calibration done
16 16:03:42 yst.200904.a400 20 PROTON yst + + - + + + + LBP-1 sref: reference peak not found default calibration done
6 15:01:51 lss.200904.a400 10 PROTON lss + + - + + + + LSS-15 pure
5 12:01:29 ms.200904.a400 10 PROTON ms + + - + + + + BODIPY-CN column sref: reference peak not found default calibration done
1 11:44:04 cyl.200904.a400 10 PROTON cyl + + - + + + + MCD_CL-02-48-1-1
24 11:37:15 ki407_6.200904.a400 10 PROTON ki + + - + + + + KI 407-6 sref: reference peak not found default calibration done
18 11:26:40 gg.200904.a400 10 PROTON gg + + - - + + + GG01-88_Product
13 11:18:43 ial_37_1b.200904.a400 10 PROTON ial + + - - + + +
12 11:09:48 ial_37_1a.200904.a400 10 PROTON ial + + - + + + +
20 10:52:55 naa.200904.a400 10 PROTON naa + + - + + + + NAA72
11 10:45:15 yst.200904.a400 10 PROTON yst + + - + + + + 2,6-DiCl benzoic acid sref: reference peak not found default calibration done
6 10:32:15 ed.200904.a400 10 PROTON ed + + - + + + + ED_THIOPHENPINACOLESTER_VASKET_FOER KOLONNE
23 10:04:32 gb.200904.a400 10 PROTON gb + + - + + + + GB-15-1 sref: reference peak not found default calibration done
5 09:45:24 jop.200904.a400 12 F19CPD_KU jop - + - - - + + jop_v_213_1
5 09:29:24 jop.200904.a400 11 C13 jop - + - - - + + jop_v_213_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 09:21:42 jop.200904.a400 10 PROTON jop + + - - + + + jop_v_213_1 sref: reference peak not found default calibration done
10 09:13:13 fr.200904.a400 20 PROTON fr + + - + + + + FR-117-1A
11 08:14:05 fr.200904.a400 10 F19CPD_KU fr + + - + + + + FR-116-1C - F19 WITH DECOUPLING
21 00:09:23 mef.200903.a400 21 C13CPD mef + + - - + + + MEF100-pure? sref: reference peak not found default calibration done
20 23:04:17 mef.200903.a400 11 C13CPD mef + + - + + + + MEF100-DCM-MeOH sref: reference peak not found default calibration done
13 22:00:05 ap.200903.a400 43 C13CPD ap + + - + + + + 7-24_crude sref: reference peak not found default calibration done
4 19:53:36 jop.200903.a400 31 C13 jop - + - - - + + jop_v_212_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
4 19:48:00 jop.200903.a400 30 PROTON jop + + - - x + + jop_v_212_1 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
14 19:13:03 av.200903.a400 11 C13 av + + - - + + + 85 purif au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
21 19:08:12 mef.200903.a400 20 PROTON mef + + - - x + + MEF100-pure? topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
20 19:00:01 mef.200903.a400 10 PROTON mef + + - + + + + MEF100-DCM-MeOH
13 18:39:14 ap.200903.a400 42 HSQC ap + + - + + + + 7-24_crude
14 18:31:55 av.200903.a400 10 PROTON av + + - + + + + 85 purif sref: reference peak not found default calibration done
13 18:29:19 ap.200903.a400 41 P31CPD ap - + - - - + + 7-24_crude
13 18:18:31 ap.200903.a400 40 PROTON ap + + - + + + + 7-24_crude sref: reference peak not found default calibration done
17 17:41:49 at3_5_1.200903.a400 10 PROTON at + + - + + + +
23 16:46:33 gb.200903.a400 20 PROTON gb + + - - + + + GB-15-1crudesecondspot sref: reference peak not found default calibration done
24 16:39:25 gb.200903.a400 10 PROTON gb + + - - + + + GB-15-1crudeterzospot sref: reference peak not found default calibration done
22 16:31:45 lss.200903.a400 10 PROTON lss + + - + + + + LSS-13 tBu
2 15:54:35 aog_002.200903.a400 10 PROTON aog + + - - + + + sref: reference peak not found default calibration done
4 15:47:57 umbJ1.200903.a400 10 PROTON umb + + - + x + + topshim: FieldMap - no valid data in sample centre, Shim failed, sref: reference peak not found default calibration done
22 14:59:39 fr.200903.a400 10 PROTON fr + + - - + + + FR-116-1C - HNMR
16 14:52:32 ms.200903.a400 10 PROTON ms + + - - + + + BODIPY col wash sref: reference peak not found default calibration done
7 14:44:24 par.200903.a400 20 PROTON par + + - - x + + 100-009-s50 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
8 14:34:45 par.200903.a400 10 PROTON par + + - + + + + 100-009-pure
13 14:32:51 ap.200903.a400 31 P31CPD ap - + - - - + + 7-21_f3,4
13 14:24:19 ap.200903.a400 30 PROTON ap + + - - + + + 7-21_f3,4
14 14:22:24 ap.200903.a400 21 P31CPD ap - + - - - + + 7-21_f14
14 14:11:53 ap.200903.a400 20 PROTON ap + + - - + + + 7-21_f14
10 14:09:43 ap.200903.a400 11 P31CPD ap - + - - - + + 7-21_f6
10 13:58:36 ap.200903.a400 10 PROTON ap + + - + + + + 7-21_f6
1 13:42:53 jop.200903.a400 21 C13 jop - + - - - + + jop_v_211_1_2 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 13:35:09 jop.200903.a400 20 PROTON jop + + - + + + + jop_v_211_1_2 sref: reference peak not found default calibration done
3 11:40:25 ed.200903.a400 10 PROTON ed + + - + + + + emil_thiophenpinacole_EP1_filtrat (90grader)
8 10:17:34 umbnos.200903.a400 10 PROTON umb + + - + + + +
6 10:09:52 aln.200903.a400 20 WATER aln + + - - + + + ALN-306_EnzymeRes_on sref: reference peak not found default calibration done
5 10:02:09 aln.200903.a400 10 WATER aln + + - + + + + ALN-306_RM sref: reference peak not found default calibration done
2 09:26:15 jop.200903.a400 11 C13 jop - + - - - + + jop_v_212_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 09:18:45 jop.200903.a400 10 PROTON jop + + - + + + + jop_v_212_1 sref: reference peak not found default calibration done
13 18:44:45 av.200902.a400 20 PROTON av + + - + + + + AV1-85 crude
21 18:37:40 yd.200902.a400 40 PROTON yd + + - + + + + YD-600-197-crude in DMSO sref: reference peak not found default calibration done
20 18:30:34 yd.200902.a400 30 PROTON yd + + - - + + + YD-600-197-crude in CDCl3
19 18:22:07 ial_39_1b.200902.a400 10 PROTON ial + + - - + + +
18 18:13:31 ial_39_1a.200902.a400 10 PROTON ial + + - + + + +
15 18:05:06 yst.200902.a400 50 PROTON yst + + - - + + + VF-19 De-H DCl
11 18:03:11 ap.200902.a400 81 P31CPD ap - + - - - + + 7-20_f8
11 17:52:51 ap.200902.a400 80 PROTON ap + + - - + + + 7-20_f8
10 17:50:36 ap.200902.a400 71 P31CPD ap - + - - - + + 7-20_f7
10 17:39:27 ap.200902.a400 70 PROTON ap + + - + + + + 7-20_f7
1 17:23:37 jop.200902.a400 11 C13 jop - + - - - + + JOP_V_211_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 17:16:16 jop.200902.a400 10 PROTON jop + + - + + + + JOP_V_211_1 sref: reference peak not found default calibration done
12 16:23:43 naa.200902.a400 11 C13 naa - + - - - + + NAA66 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
12 16:16:22 naa.200902.a400 10 PROTON naa + + - + + + + NAA66
16 15:19:15 fr.200902.a400 20 PROTON fr + + - + + + + FR-116-1B
8 15:11:24 yst.200902.a400 40 PROTON yst + + - - + + + VF-19 De-H AcOH sref: reference peak not found default calibration done
7 15:03:35 yst.200902.a400 30 PROTON yst + + - - + + + VF-19 De-H TFA
6 14:55:34 yst.200902.a400 20 PROTON yst + + - - + + + VF-19 De-H HCl
5 14:47:24 yst.200902.a400 10 PROTON yst + + - + + + + VF-19 De-H CD3OD
17 14:42:11 yeAOG001.200902.a400 10 PROTON ye + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
14 14:12:08 cpo628.200902.a400 11 C13 cpo - + - - - + + CPO628-204 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
14 14:04:36 cpo628.200902.a400 10 PROTON cpo + + - - + + + CPO628-204
23 13:29:18 at3_1_6.200902.a400 11 C13APT_KU at + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 12:54:27 yd.200902.a400 20 PROTON yd + + - - + + + YD-515-198-crude in d2o sref: reference peak not found default calibration done
1 12:47:59 yd.200902.a400 10 PROTON yd + + - + + + + YD-601-191-pure in d2o sref: reference peak not found default calibration done
23 12:03:21 at3_1_6.200902.a400 10 PROTON at + + - + + + +
13 11:45:35 av.200902.a400 11 C13 av - + - - - + + AV1-84 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
13 11:38:39 av.200902.a400 10 PROTON av + + - + + + + AV1-84
10 11:20:00 cpo630.200902.a400 10 PROTON cpo + + - + + + + CPo630-207 crude
13 11:17:35 ap.200902.a400 61 P31CPD ap - + - - - + + 7-21_f11
13 11:06:20 ap.200902.a400 60 PROTON ap + + - + + + + 7-21_f11
10 10:54:26 fr.200902.a400 10 PROTON fr + + - + + + + FR-116-1A
15 10:52:31 ap.200902.a400 51 P31CPD ap - + - - - + + 7-21_f10
15 10:42:03 ap.200902.a400 50 PROTON ap + + - - + + + 7-21_f10
14 10:40:07 ap.200902.a400 41 P31CPD ap - + - - - + + 7-21_f9
14 10:29:34 ap.200902.a400 40 PROTON ap + + - - + + + 7-21_f9
13 10:27:37 ap.200902.a400 31 P31CPD ap - + - - - + + 7-21_f5
13 10:16:42 ap.200902.a400 30 PROTON ap + + - - + + + 7-21_f5 sref: reference peak not found default calibration done
15 10:14:45 ap.200902.a400 21 P31CPD ap - + - - - + + 7-21_f13
15 10:04:33 ap.200902.a400 20 PROTON ap + + - - + + + 7-21_f13 sref: reference peak not found default calibration done
14 10:02:19 ap.200902.a400 11 P31CPD ap - + - - - + + 7-21_f12
14 09:51:25 ap.200902.a400 10 PROTON ap + + - + + + + 7-21_f12 sref: reference peak not found default calibration done
17 09:39:40 cvh.200902.a400 10 PROTON cvh + + - + + + + CVI1-59
24 00:49:40 atapeiro.200901.a400 10 PROTON at + + - - + + +
23 00:43:31 at47_apeiro.200901.a400 10 PROTON at + + - - + + +
22 00:37:31 at40_46.200901.a400 10 PROTON at + + - - + + +
20 00:30:51 at24_29.200901.a400 10 PROTON at + + - - + + +
21 00:24:18 at30_35.200901.a400 10 PROTON at + + - - + + +
19 00:17:50 at9_24.200901.a400 10 PROTON at + + - - + + +
18 00:10:06 at1_4.200901.a400 10 PROTON at + + - + + + +
10 23:05:52 gg.200901.a400 13 C13CPD gg + + - + + + + GG01-73.2_A4 sref: reference peak not found default calibration done
4 22:01:41 jmr.200901.a400 11 C13CPD jmr + + - + + + + sref: reference peak not found default calibration done
3 18:26:37 jn234cru.200901.a400 10 PROTON jn + + - - + + + jn234cru
17 18:05:53 av.200901.a400 11 C13 av + + - + + + + AV1-84 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
6 18:00:02 bhgMercap.200901.a400 11 COSY bhg - + - - - + +
6 17:53:08 bhgMercap.200901.a400 10 PROTON bhg + + - + + + + sref: reference peak not found default calibration done
17 17:45:45 av.200901.a400 10 PROTON av + + - + + + + AV1-84 sref: reference peak not found default calibration done
24 16:44:21 yst.200901.a400 70 PROTON yst + + - + + + + VF-19 deprotonation test 5h
3 16:36:14 cpo629.200901.a400 10 PROTON cpo + + - + + + + CPO629-206 crude
16 14:36:27 fba.200901.a400 40 PROTON fba + + - + + + + FB-101-1.1FF sref: reference peak not found default calibration done
15 14:29:51 fba.200901.a400 30 PROTON fba + + - + + + + FB-102-1.1 sref: reference peak not found default calibration done
22 14:13:21 ial_37_1.200901.a400 20 PROTON ial + + - + + + + sref: reference peak not found default calibration done
2 13:57:38 jop.200901.a400 31 C13 jop - + - - - + + jop_v_210_2 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 13:50:24 jop.200901.a400 30 PROTON jop + + - + + + + jop_v_210_2 sref: reference peak not found default calibration done
3 13:40:21 fr.200901.a400 21 COSY fr - + - - - + + FR-115-1B - HNMR COSY
3 13:30:33 fr.200901.a400 20 PROTON fr + + - + + + + FR-115-1B - HNMR
8 13:23:11 fba.200901.a400 20 PROTON fba + + - + + + + FB-101-1.1F sref: reference peak not found default calibration done
24 13:15:14 yst.200901.a400 60 PROTON yst + + - - + + + VF-19 deprotonation 1h
19 13:06:31 yst.200901.a400 50 PROTON yst + + - + + + + VF-19 deprotonation 30 min
22 12:58:15 ial_37_1.200901.a400 10 PROTON ial + + - - + + + sref: reference peak not found default calibration done
21 12:50:06 ial_38_1cdcl.200901.a400 10 PROTON ial + + - + + + +
20 12:41:54 ial_38_1dmso.200901.a400 10 PROTON ial + + - + + + + sref: reference peak not found default calibration done
18 12:34:51 fba.200901.a400 10 PROTON fba + + - + + + + FB-101-1.1S sref: reference peak not found default calibration done
17 12:26:59 yst.200901.a400 40 PROTON yst + + - - + + + VF-19 deprotonation 20 min
16 12:19:03 yst.200901.a400 30 PROTON yst + + - - + + + VF-19 deprotonation 10 min
15 12:11:13 yst.200901.a400 20 PROTON yst + + - - + + + VF-19 deprotonation 5 min
14 12:02:01 yst.200901.a400 10 PROTON yst + + - + + + + VF-19 deprotonation 0min
7 11:46:01 jop.200901.a400 21 C13 jop - + - - - + + jop_v_210_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
7 11:40:46 jop.200901.a400 20 PROTON jop + + - - x + + jop_v_210_1 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
1 11:38:21 jop.200901.a400 12 F19CPD_KU jop - + - - - + + jop_V_205_1
1 11:22:34 jop.200901.a400 11 C13 jop - + - - - + + jop_V_205_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 11:15:02 jop.200901.a400 10 PROTON jop + + - + + + + jop_V_205_1 sref: reference peak not found default calibration done
20 11:02:19 atwater.200901.a400 10 PROTON at + x - + + + + ATM Failed, sref: reference peak not found default calibration done
22 10:50:56 cpo.200901.a400 10 PROTON cpo + + - + + + + MEF30 - check sref: reference peak not found default calibration done
10 10:20:13 gg.200901.a400 12 HSQC gg - + - - - + + GG01-73.2_A4
10 10:14:22 gg.200901.a400 11 COSY gg - + - - - + + GG01-73.2_A4
10 09:58:36 gg.200901.a400 10 PROTON gg + + - + + + + GG01-73.2_A4 sref: reference peak not found default calibration done
4 09:36:03 jmr.200901.a400 10 PROTON jmr + + - + + + +
8 07:56:16 fr.200901.a400 10 PROTON fr + + - + + + + FR-115-1A - HNMR
13 03:46:21 em.200831.a400 43 HSQC em - + - - - + + 72d
13 03:26:03 em.200831.a400 42 COSY em - + - - - + + 72d
13 02:22:19 em.200831.a400 41 C13CPD em + + - - + + + 72d sref: reference peak not found default calibration done
12 02:06:55 em.200831.a400 33 HSQC em - + - - - + + 24d
12 01:02:46 em.200831.a400 32 C13CPD em + + - - + + + 24d sref: reference peak not found default calibration done
11 23:04:24 em.200831.a400 24 C13CPD em - + - - - + + 24f1 sref: reference peak not found default calibration done
11 22:02:11 em.200831.a400 23 HSQC em + + - + + + + 24f1
20 21:54:52 jn242.200831.a400 10 PROTON jn + + - + + + + jn242
19 21:47:55 jn241i.200831.a400 10 PROTON jn + + - + + + + jn241i sref: reference peak not found default calibration done
5 19:28:26 gb.200831.a400 10 PROTON gb + + - + + + + GB-15-1CRUDE
8 17:17:39 ap.200831.a400 31 P31CPD ap - + - - - + +
8 17:06:33 ap.200831.a400 30 PROTON ap + + - + + + + 7-20_3rd FCC_F2
18 16:48:14 cvh.200831.a400 40 PROTON cvh + + - - x + + CVI1-39 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
17 16:40:42 cvh.200831.a400 30 PROTON cvh + + - + + + + CVI1-52
8 16:26:08 ap.200831.a400 21 P31CPD ap - + - - - + +
8 16:15:23 ap.200831.a400 20 PROTON ap + + - + + + + 7-20_3rd FCC_F1
21 15:27:37 fr.200831.a400 20 PROTON fr + + - + + + + cyclohexyl boronic acid
23 13:39:00 ial_cdcl3.200831.a400 10 PROTON ial + + - - + + +
20 13:23:10 cpo627.200831.a400 11 C13 cpo - + - - - + + CPO627 Fr 32-33 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
20 13:16:07 cpo627.200831.a400 10 PROTON cpo + + - - + + + CPO627 Fr 32-33
10 13:06:48 ial_38_1.200831.a400 20 PROTON ial + + - + + + +
5 12:59:12 mef.200831.a400 10 PROTON mef + + - + + + + MEF99_IMPURITY sref: reference peak not found default calibration done
8 12:43:23 fy.200831.a400 11 C13 fy - + - - - + + TFA (FY) au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 12:35:04 fy.200831.a400 10 PROTON fy + + - + + + + TFA (FY) sref: reference peak not found default calibration done
6 12:15:05 ed.200831.a400 10 PROTON ed + + - + + + + Emil, Thioester, recrystalization
4 11:56:28 yd.200831.a400 40 PROTON yd + + - + + + + YD-600-138-recrystalization in DCM (remaining)
3 11:49:39 yd.200831.a400 30 PROTON yd + + - + + + + YD-600-138-crude in DMSO sref: reference peak not found default calibration done
2 11:43:15 yd.200831.a400 20 PROTON yd + + - - + + + YD-600-138-crude in D2O sref: reference peak not found default calibration done
1 11:36:43 yd.200831.a400 10 PROTON yd + + - + + + + YD-arginine in D2O sref: reference peak not found default calibration done
19 10:34:48 lss.200831.a400 20 PROTON lss + + - + x + + ald chcl3 topshim: PerformShimming - too many points lost during fit, Shim failed
18 10:27:54 lss.200831.a400 10 PROTON lss + + - + + + + ald meoh
16 10:06:31 ial_38_1.200831.a400 10 PROTON ial + + - + + + +
14 09:38:39 cvh.200831.a400 20 PROTON cvh + + - - x + + CVI1-56 6-11 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
15 09:28:15 cvh.200831.a400 10 PROTON cvh + + - - + + + CVI1-57 7-11
22 09:21:17 fr.200831.a400 10 F19CPD_KU fr + + - + + + + FR-113-1B F19 WITH DECOUPLING
17 09:10:04 ap.200831.a400 10 PROTON ap + + - + + + + 7-20_F1_FCC_F3_2 days in MeOD
13 08:55:36 em.200831.a400 40 PROTON em + + - - x + + 72d topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
12 08:49:48 em.200831.a400 31 COSY em - + - - - + + 24d
12 08:34:24 em.200831.a400 30 PROTON em + + - - + + + 24d sref: reference peak not found default calibration done
11 08:14:12 em.200831.a400 22 COSY em - + - - - + + 24f1
11 07:58:25 em.200831.a400 21 C13 em - + - - - + + 24f1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 07:42:27 em.200831.a400 20 PROTON em + + - - + + + 24f1 sref: reference peak not found default calibration done
9 06:44:48 em.200831.a400 13 HSQC em - + - - - + + 116
9 06:24:32 em.200831.a400 12 COSY em - + - - - + + 116
9 05:20:56 em.200831.a400 11 C13CPD em + + - + + + + 116 sref: reference peak not found default calibration done; pp: Unable to assign a peak for scaling of E:/current_data/data/em/nmr/em.200831.a400/11/pdata/1/peaks No peak is found in the specified ranges!
9 01:07:43 em.200831.a400 10 PROTON em + + - + + + + 116 sref: reference peak not found default calibration done
7 13:36:41 em.200830.a400 20 PROTON em + + - + + + + 24f2ab_ppt
6 13:20:29 em.200830.a400 10 PROTON em + + - + + + + 24f2ab_ppt sref: reference peak not found default calibration done
24 14:18:33 ms090cr.200829.a400 10 PROTON ms + + - + + + + MS1028-090 crude
20 01:21:47 ap.200828.a400 71 P31CPD ap - + - - - + + 7-20_F1 FCC_F5 (f21-22)
20 01:11:26 ap.200828.a400 70 PROTON ap + + - - + + + 7-20_F1 FCC_F5 (f21-22)
18 01:09:29 ap.200828.a400 61 P31CPD ap - + - - - + + 7-20_F1 FCC_F3 (f16-21, 23-27)
18 01:01:15 ap.200828.a400 60 PROTON ap + + - - + + + 7-20_F1 FCC_F3 (f16-21, 23-27)
19 00:59:18 ap.200828.a400 51 P31CPD ap - + - - - + + 7-20_F1_FCC_F4 (f28-36)
19 00:48:34 ap.200828.a400 50 PROTON ap + + - - + + + 7-20_F1_FCC_F4 (f28-36)
17 00:46:20 ap.200828.a400 41 P31CPD ap - + - - - + + 7-20_F1_FCC_F2 (f9-15)
17 00:35:44 ap.200828.a400 40 PROTON ap + + - - + + + 7-20_F1_FCC_F2 (f9-15)
16 23:35:52 ap.200828.a400 33 C13CPD ap - + - - - + + 7-20_F1_FCC_F1 (f5,6) sref: reference peak not found default calibration done
16 23:20:10 ap.200828.a400 32 HSQC ap - + - - - + + 7-20_F1_FCC_F1 (f5,6)
16 23:17:54 ap.200828.a400 31 P31CPD ap - + - - - + + 7-20_F1_FCC_F1 (f5,6)
16 23:06:27 ap.200828.a400 30 PROTON ap + + - + + + + 7-20_F1_FCC_F1 (f5,6)
8 22:01:21 pd.200828.a400 21 C13CPD pd + + - + + + + PD3-249A sref: reference peak not found default calibration done
10 19:11:12 gg.200828.a400 10 PROTON gg + + - + + + + GG01-83_Solid sref: reference peak not found default calibration done
8 17:56:36 pd.200828.a400 20 PROTON pd + + - + + + + PD3-249A
5 17:42:08 gb.200828.a400 10 PROTON gb + + - + + + + GB-13-1-CRUDE sref: reference peak not found default calibration done
7 16:14:12 ap.200828.a400 20 F19CPD_KU ap + + - - + + + 7-23_referenced with TFA 0.01M
6 16:06:53 ap.200828.a400 21 F19CPD_KU ap + + - + + + + 7-22_reference with TFA 0.1 M
20 15:38:58 fr.200828.a400 30 PROTON fr + + - + + + + FR-114-1A - HNMR
14 14:59:06 ap.200828.a400 11 F19CPD_KU ap - + - - - + + TFA reference 0.1 M in CDCl3
14 14:52:02 ap.200828.a400 10 PROTON ap + + - + + + + TFA reference 0.1 M in CDCl3
3 14:34:12 ed.200828.a400 20 PROTON ed + + - + + + + Emil, thiophen ester, vasket
4 13:41:52 pd.200828.a400 10 PROTON pd + + - + + + + PD3-233CR sref: reference peak not found default calibration done
2 13:29:06 ed.200828.a400 10 PROTON ed + + - - + + + Thiophene, esterfication. No work-up
11 13:13:18 cpo627.200828.a400 11 C13 cpo - + - - - + + CPO627-202 crude au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 13:05:52 cpo627.200828.a400 10 PROTON cpo + + - + + + + CPO627-202 crude
1 11:42:17 mef.200828.a400 11 C13 mef - + - - - + + MEF99_pure_CC au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 11:35:29 mef.200828.a400 10 PROTON mef + + - + + + + MEF99_pure_CC sref: reference peak not found default calibration done
24 10:50:58 fr.200828.a400 21 COSY fr - + - - - + + FR-113-1B - HNMR COSY
24 10:42:37 fr.200828.a400 20 PROTON fr + + - + + + + FR-113-1B - HNMR
19 08:11:14 fr.200828.a400 10 PROTON fr + + - + + + + FR-113-1A - HNMR
14 04:53:35 ap.200827.a400 42 F19CPD_KU ap - + - - - + + 7-23_F1
14 04:51:03 ap.200827.a400 41 P31CPD ap - + - - - + + 7-23_F1 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200827.a400/41/pdata/1/peaks!
14 04:32:40 ap.200827.a400 40 PROTON ap + + - + + + + 7-23_F1
11 00:32:25 cpo621.200827.a400 11 C13CPD cpo + + - + + + + CPO621-ReCryst (HCL) sref: reference peak not found default calibration done
9 23:27:24 em.200827.a400 11 C13CPD em + + - + + + + 157HEf98-109 sref: reference peak not found default calibration done
14 23:06:06 ap.200827.a400 43 HSQC ap + + - + + + + 7-23_F1
23 22:01:16 ap.200827.a400 23 C13CPD ap + + - + + + + 7-20_F3 sref: reference peak not found default calibration done
5 19:29:29 ktt.200827.a400 10 PROTON ktt + + - + + + + sref: reference peak not found default calibration done
2 18:20:55 yd.200827.a400 10 PROTON yd + + - + + + + YD-513-195-pure
23 17:49:34 ap.200827.a400 22 HSQC ap + + - + + + + 7-20_F3
9 17:38:10 em.200827.a400 10 PROTON em + + - + + + + 157HEf98-109 sref: reference peak not found default calibration done
24 17:35:55 ap.200827.a400 31 P31CPD ap - + - - - + + 7-20_F2
24 17:29:24 ap.200827.a400 30 PROTON ap + + - + + + + 7-20_F2
12 16:59:44 cpo621.200827.a400 20 PROTON cpo + + - - + + + CPO621-ML (HCL)
11 16:52:33 cpo621.200827.a400 10 PROTON cpo + + - + + + + CPO621-ReCryst (HCL) sref: reference peak not found default calibration done
8 16:44:43 gg.200827.a400 10 PROTON gg + + - + + + + GG01-83_hydrolysis_product sref: reference peak not found default calibration done
22 15:25:04 ap.200827.a400 12 HSQC ap + + - - + + + 7-20_F1
23 15:23:06 ap.200827.a400 21 P31CPD ap - + - - - + + 7-20_F3
23 15:16:33 ap.200827.a400 20 PROTON ap + + - - + + + 7-20_F3
22 15:14:18 ap.200827.a400 11 P31CPD ap - + - - - + + 7-20_F1
22 15:03:33 ap.200827.a400 10 PROTON ap + + - + + + + 7-20_F1
13 14:52:12 ms089c.200827.a400 10 PROTON ms + + - + + + + MS1036-089 column
10 12:09:38 ms089cr.200827.a400 10 PROTON ms + + - - + + + MS1036-089 crude
7 12:01:05 fr.200827.a400 10 PROTON fr + + - + + + + 4-Br-BnBr - hmr
1 10:50:01 mef.200827.a400 11 C13 mef - + - - - + + MEF99 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 10:42:55 mef.200827.a400 10 PROTON mef + + - + + + + MEF99 sref: reference peak not found default calibration done
20 10:34:48 ial_37_1.200827.a400 10 PROTON ial + + - + + + +
18 09:32:49 ays.200827.a400 10 PROTON ays + + - + + + + BocHNCH2CHO-D-Lys(CbzG)-COAllyl(Crude)
14 00:09:11 em.200826.a400 11 C13CPD em + + - - + + + 147lefts_DMF sref: reference peak not found default calibration done
6 23:05:59 ap.200826.a400 33 C13CPD ap + + - - x + + 7-22_F1 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
9 22:01:11 em.200825.a400 11 C13CPD em + + - + + + + 156wu
21 21:19:26 em.200826.a400 21 PROTON em - + - - - + + 147lefts_2 sref: reference peak not found default calibration done
21 21:13:14 em.200826.a400 20 PROTON em + + - + + + + 147lefts_2 sref: reference peak not found default calibration done
18 19:47:59 gg.200826.a400 20 PROTON gg + + - - x + + GG01-67_Ext_Org topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
17 19:39:46 gg.200826.a400 10 PROTON gg + + - + + + + GG01-67_Solid
14 19:04:00 em.200826.a400 10 PROTON em + + - + + + + 147lefts_DMF
23 18:54:46 ap.200826.a400 41 F19CPD_KU ap - + - - - + + 7-22_F3 (f28-48)
23 18:43:32 ap.200826.a400 40 PROTON ap + + - + + + + 7-22_F3 (f28-48)
13 17:48:38 par.200826.a400 50 PROTON par + + - + + + + 104-002 sref: reference peak not found default calibration done
12 17:41:42 par.200826.a400 40 PROTON par + + - + + + + 100-009-cc
6 16:52:43 ap.200826.a400 33 HSQC ap + + - - + + + 7-22_F1
5 16:46:25 ays.200826.a400 10 PROTON ays + + - - x + + BocHN-CH2-CHO topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
24 16:37:07 fr.200826.a400 20 PROTON fr + + - + + + + FR-107-1C - HNMR
3 16:34:59 pd.200826.a400 11 P31CPD pd - + - - - + + PD-230A
3 16:23:35 pd.200826.a400 10 PROTON pd + + - + + + + PD-230A
2 16:11:37 ed.200826.a400 10 PROTON ed + + - + + + + Emil_Suzuki_Cyano int., small scale
11 16:00:13 ial_38_1b.200826.a400 10 PROTON ial + + - - + + +
10 15:51:45 ial_38_1a.200826.a400 10 PROTON ial + + - + + + +
22 15:41:41 cpo621.200826.a400 20 PROTON cpo + + - - + + + CPO621-205 ML
21 15:25:07 cpo621.200826.a400 10 PROTON cpo + + - + + + + CPO621-205 Residue
6 15:22:48 ap.200826.a400 32 F19CPD_KU ap - + - - - + + 7-22_F1
6 15:20:41 ap.200826.a400 31 P31CPD ap - + - - - + + 7-22_F1
6 15:03:22 ap.200826.a400 30 PROTON ap + + - + + + + 7-22_F1
18 14:13:53 jiz.200826.a400 20 PROTON jiz + + - - + + + 42121 sref: reference peak not found default calibration done
17 14:07:27 jiz.200826.a400 10 PROTON jiz + + - + + + + 42112 sref: reference peak not found default calibration done
8 13:27:21 par.200826.a400 30 PROTON par + + - + + + + 104-002-CC sref: reference peak not found default calibration done
7 12:45:23 par.200826.a400 20 PROTON par + + - + + + + 103-002
24 11:24:12 fr.200826.a400 11 COSY fr - + - - - + + FR-107-1B - COSY
24 11:15:09 fr.200826.a400 10 PROTON fr + + - + + + + FR-107-1B - HNMR
16 10:36:10 par.200826.a400 10 PROTON par + + - + + + + 102-003-pure
24 10:34:14 ap.200826.a400 21 P31CPD ap - + - - - + + 7-21_crude
24 10:23:28 ap.200826.a400 20 PROTON ap + + - - + + + 7-21_crude
23 10:21:14 ap.200826.a400 11 P31CPD ap - + - - - + + 7-20_crude
23 10:10:36 ap.200826.a400 10 PROTON ap + + - + + + + 7-20_crude
18 07:01:01 gg.200825.a400 23 C13CPD gg + + - - + + + GG01-73_F#669-GG-A4 sref: reference peak not found default calibration done
19 06:15:07 jiz.200825.a400 14 HMBC_LP jiz - + - - - + +
19 05:59:43 jiz.200825.a400 13 HSQC jiz - + - - - + +
19 05:53:55 jiz.200825.a400 12 COSY jiz - + - - - + +
19 22:01:06 jiz.200825.a400 11 C13CPD jiz + + - + + + + sref: reference peak not found default calibration done
19 21:18:12 jiz.200825.a400 10 PROTON jiz + + - + + + + sref: reference peak not found default calibration done
15 20:16:43 gg.200825.a400 30 PROTON gg + + - + + + + GG01-81_Product
11 19:05:59 jn058x2.200825.a400 10 PROTON jn + + - + + + + jn058x2
4 18:38:57 kov.200825.a400 10 PROTON kov + + - + + + + KOV01-110 sref: reference peak not found default calibration done
9 18:18:58 em.200825.a400 10 PROTON em + + - + + + + 156wu
1 16:54:03 par.200825.a400 20 PROTON par + + - + + + + 100-009-i sref: reference peak not found default calibration done
13 15:34:08 lss.200825.a400 10 PROTON lss + + - + + + + Ald crude
10 15:20:00 cvh.200825.a400 10 PROTON cvh + + - + + + + CVI1-52
8 14:07:42 jn238x1.200825.a400 11 C13 jn - + - - - + + jn238x1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 14:00:55 jn238x1.200825.a400 10 PROTON jn + + - + + + + jn238x1
20 13:42:23 ial_36_1.200825.a400 10 PROTON ial + + - + + + +
18 11:53:03 gg.200825.a400 22 HSQC gg + + - + + + + GG01-73_F#669-GG-A4
12 11:41:50 par.200825.a400 10 PROTON par + + - - + + + 102-003-funnel sref: reference peak not found default calibration done
7 11:35:09 jneredf5_12.200825.a400 10 PROTON jn + + - - + + + jneredf5_12
6 11:30:18 jn314f3_4.200825.a400 10 PROTON jn + + - - x + + jn314f3_4 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
5 11:22:55 jn235hclx1.200825.a400 10 PROTON jn + + - + + + + jn235hclx1
18 11:17:07 gg.200825.a400 21 COSY gg - + - - - + + GG01-73_F#669-GG-A4
18 11:01:17 gg.200825.a400 20 PROTON gg + + - + + + + GG01-73_F#669-GG-A4 sref: reference peak not found default calibration done
10 10:24:42 gg.200825.a400 12 HSQC gg - + - - - + + GG01-73
10 10:18:53 gg.200825.a400 11 COSY gg - + - - - + + GG01-73
10 10:12:47 gg.200825.a400 10 PROTON gg + + - + + + + GG01-73 sref: reference peak not found default calibration done
3 19:37:00 yd.200824.a400 10 PROTON yd + + - + + + + YD-514-192-crude
1 17:07:01 pd.200824.a400 21 P31CPD pd - + - - - + + PD-241C
1 16:56:12 pd.200824.a400 20 PROTON pd + + - + + + + PD-241C
22 16:43:04 gb.200824.a400 20 PROTON gb + + - + + + + GB-10-1-3spot
5 16:16:26 gb.200824.a400 10 PROTON gb + + - + + + + GB-10-1-2ndspot sref: reference peak not found default calibration done
12 15:47:33 jn236cru.200824.a400 10 PROTON jn + + - + + + + jn236cru
9 15:05:10 ial_29_1.200824.a400 10 PROTON ial + + - + + + + sref: reference peak not found default calibration done
7 14:54:46 pd.200824.a400 11 P31CPD pd - + - - - + + PD-241B
7 14:46:35 pd.200824.a400 10 PROTON pd + + - + + + + PD-241B
7 11:45:10 fr.200824.a400 30 PROTON fr + + - + + + + FR-107-1A - HNMR
20 11:40:23 ap.200824.a400 21 F19CPD_KU ap - + - - - + + 7-18
20 11:29:05 ap.200824.a400 20 PROTON ap + + - + + + + 7-18
8 11:09:57 cvh.200824.a400 10 PROTON cvh + + - - + + + CVI1-52 3-9
2 11:02:23 asma.200824.a400 10 PROTON asma + + - + + + + AM2-80-1 sref: reference peak not found default calibration done
7 10:27:35 ap.200824.a400 11 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f6-11
7 10:16:38 ap.200824.a400 10 PROTON ap + + - + + + + 7-16_2nd Reveleris_f6-11
24 10:10:54 fr.200824.a400 21 COSY fr - + - - - + + FR-108-1G - COSY
24 10:00:19 fr.200824.a400 20 PROTON fr + + - - + + + FR-108-1G - HNMR
18 09:52:35 ial_35_1a.200824.a400 10 PROTON ial + + - - + + +
17 09:44:38 ial_35_1c.200824.a400 10 PROTON ial + + - + + + +
12 08:13:43 fr.200824.a400 10 PROTON fr + + - + + + + FR-108-1F - SAMPLE 2
22 16:54:54 ap.200823.a400 92 F19CPD_KU ap - + - - - + + 7-16_F1
22 16:52:49 ap.200823.a400 91 P31CPD ap - + - - - + + 7-16_F1
22 16:41:46 ap.200823.a400 90 PROTON ap + + - + + + + 7-16_F1
23 16:03:02 ap.200823.a400 82 F19CPD_KU ap - + - - - + + 7-16_F2
23 16:01:07 ap.200823.a400 81 P31CPD ap - + - - - + + 7-16_F2
23 15:50:14 ap.200823.a400 80 PROTON ap + + - + + + + 7-16_F2
20 14:44:28 jn236_210.200823.a400 10 PROTON jn + + - + + + + jn236_210
12 14:27:31 ap.200823.a400 71 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f12
12 14:17:19 ap.200823.a400 70 PROTON ap + + - - + + + 7-16_2nd Reveleris_f12
10 14:15:24 ap.200823.a400 61 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f13-14
10 14:04:44 ap.200823.a400 60 PROTON ap + + - - + + + 7-16_2nd Reveleris_f13-14
11 14:02:48 ap.200823.a400 51 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f15
11 13:51:27 ap.200823.a400 50 PROTON ap + + - - + + + 7-16_2nd Reveleris_f15
12 13:49:29 ap.200823.a400 41 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f20-21
12 13:38:05 ap.200823.a400 40 PROTON ap + + - + + + + 7-16_2nd Reveleris_f20-21
22 13:30:34 jn236_120.200823.a400 10 PROTON jn + + - - + + + jn236_120 sref: reference peak not found default calibration done
21 13:25:25 jn236_180.200823.a400 10 PROTON jn + + - - x + + jn236_180 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
20 13:18:29 jn237_rt70.200823.a400 10 PROTON jn + + - + + + + jn237_rt70 sref: reference peak not found default calibration done
10 13:12:13 ap.200823.a400 31 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f12
10 13:00:18 ap.200823.a400 30 PROTON ap + + - + + + + 7-16_2nd Reveleris_f12 sref: reference peak not found default calibration done
11 12:58:23 ap.200823.a400 21 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f16
11 12:47:10 ap.200823.a400 20 PROTON ap + + - - + + + 7-16_2nd Reveleris_f16
12 12:44:56 ap.200823.a400 11 P31CPD ap - + - - - + + 7-16_2nd Reveleris_f17-19
12 12:33:35 ap.200823.a400 10 PROTON ap + + - + + + + 7-16_2nd Reveleris_f17-19
22 11:41:03 jn237_15dry.200823.a400 10 PROTON jn + + - + + + + jn237_15dry sref: reference peak not found default calibration done
21 11:36:09 jn237_15wet.200823.a400 10 PROTON jn + + - x - - - jn237_15wet lock: Command 'lock CDCl3' failed. Lock is OFF, Lock failed after multiple attempts, lock: Command 'lock CDCl3' failed. Lock is OFF, Command 'lock CDCl3' failed. Lock is OFF
20 11:29:36 jn236_60.200823.a400 10 PROTON jn + + - + + + + jn236_60min sref: reference peak not found default calibration done
8 22:00:51 cvh.200821.a400 12 C13CPD cvh + + - + + + + CVI1-51 7-12 sref: reference peak not found default calibration done
17 19:03:27 ap.200822.a400 91 F19CPD_KU ap - + - - - + + 7-17
17 18:51:26 ap.200822.a400 90 PROTON ap + + - + + + + 7-17
18 16:26:42 gg.200822.a400 10 PROTON gg + + - + + + + GG01-77_Product sref: reference peak not found default calibration done
12 15:42:06 ap.200822.a400 81 P31CPD ap - + - - - + + 7-19
12 15:31:35 ap.200822.a400 80 PROTON ap + + - - + + + 7-19
17 15:24:47 ap.200822.a400 70 F19CPD_KU ap + + - + + + + 7-16_f12
19 14:24:41 om_i_41.200822.a400 12 C13 om - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
19 14:14:06 om_i_41.200822.a400 11 COSY om - + - - - + +
19 14:04:31 om_i_41.200822.a400 10 PROTON om + + - + + + + sref: reference peak not found default calibration done
10 13:18:09 ap.200822.a400 61 P31CPD ap - + - - - + + 7-16_f7
10 13:06:40 ap.200822.a400 60 PROTON ap + + - - + + + 7-16_f7
11 13:04:30 ap.200822.a400 51 P31CPD ap - + - - - + + 7-16_f8
11 12:52:59 ap.200822.a400 50 PROTON ap + + - - + + + 7-16_f8
12 12:50:59 ap.200822.a400 21 P31CPD ap - + - - - + + 7-16_f9
12 12:40:20 ap.200822.a400 20 PROTON ap + + - + + + + 7-16_f9
11 12:24:19 ap.200822.a400 41 P31CPD ap - + - - - + + 7-16_f11
11 12:12:50 ap.200822.a400 40 PROTON ap + + - - + + + 7-16_f11
12 12:10:48 ap.200822.a400 31 P31CPD ap - + - - - + + 7-16_f12
12 11:54:29 ap.200822.a400 30 PROTON ap + + - - + + + 7-16_f12
10 11:52:14 ap.200822.a400 11 P31CPD ap - + - - - + + 7-16_f10
10 11:40:53 ap.200822.a400 10 PROTON ap + + - + + + + 7-16_f10
12 06:28:30 jiz.200821.a400 14 HMBC_LP jiz - + - - - + + JZ08_103
12 06:13:00 jiz.200821.a400 13 HSQC jiz - + - - - + + JZ08_103
12 06:07:07 jiz.200821.a400 12 COSY jiz - + - - - + + JZ08_103
12 02:07:26 jiz.200821.a400 11 C13CPD jiz + + - + + + + JZ08_103 sref: reference peak not found default calibration done
6 01:21:32 emjn213.200821.a400 13 HMBC_LP emr - + - - - + + jn213p oxime
6 01:06:08 emjn213.200821.a400 12 HSQC emr - + - - - + + jn213p oxime
6 00:01:37 emjn213.200821.a400 11 C13CPD emr + + - - + + + jn213p oxime sref: reference peak not found default calibration done
20 22:00:46 at3_1_5.200821.a400 10 C13APT_KU_night at + + - + + + + sref: reference peak not found default calibration done
24 19:47:49 jn136x3.200821.a400 10 PROTON jn + + - - + + + jn136x3
23 19:41:47 jn132x2.200821.a400 10 PROTON jn + + - - + + + jn132x2
22 19:34:56 jn130x1.200821.a400 10 PROTON jn + + - + + + + jn130x1 sref: reference peak not found default calibration done
21 19:28:16 jn236sm.200821.a400 10 PROTON jn + + - + + + + jn236sm sref: reference peak not found default calibration done
14 18:27:40 ial_35_1b.200821.a400 10 PROTON ial + + - + + + +
11 18:13:37 atmalakies.200821.a400 10 PROTON at + + - + + + + sref: reference peak not found default calibration done
21 17:53:35 at3_3_3.200821.a400 10 PROTON at + + - + + + +
11 17:49:45 ap.200821.a400 12 F19CPD_KU ap - + - - - + + 7-16_crude
11 17:47:33 ap.200821.a400 11 P31CPD ap - + - - - + + 7-16_crude
11 17:36:22 ap.200821.a400 10 PROTON ap + + - + + + + 7-16_crude
19 17:25:10 lss.200821.a400 20 PROTON lss + + - - + + + Cycl. 7-16
17 17:13:33 lss.200821.a400 10 PROTON lss + + - + + + + Cycl. tube 6
4 16:58:16 yd.200821.a400 10 PROTON yd - + - - - + + YD-513-192-pure
4 16:37:30 yd.200821.a400 11 C13 yd + + - + + + + YD-513-192-pure au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
13 15:43:28 fr.200821.a400 20 PROTON fr + + - + + + + FR-108-1F
8 15:33:56 cvh.200821.a400 11 PROTON cvh + + - + + + + CVI1-51 7-12
8 15:01:55 cvh.200821.a400 10 PROTON cvh + + - + x + + CVI1-51 7-12 topshim: PerformShimming - too many points lost during fit, Shim failed, sref: reference peak not found default calibration done
15 14:55:37 gg.200821.a400 10 PROTON gg + + - - + + + GG01-75_Product sref: reference peak not found default calibration done
10 14:37:14 mmsh.200821.a400 10 PROTON mmsh + + - - + + + mh01-5-5-peg-boc-cl-t5 sref: reference peak not found default calibration done
7 14:30:40 ktt.200821.a400 10 PROTON ktt + + - + + + + KTT15-169_pur sref: reference peak not found default calibration done
3 14:23:19 par.200821.a400 30 PROTON par + + - - + + + 102-003-filter paper
2 14:17:11 par.200821.a400 20 PROTON par + + - - x + + 102-003-heptane washed water phase topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
1 14:10:01 par.200821.a400 10 PROTON par + + - - + + + 102-003-water phase
6 14:02:46 emjn213.200821.a400 10 PROTON emr + + - + + + + jn213p oxime
5 13:32:50 jop.200821.a400 11 C13 jop - + - - - + + jop_V_202_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 13:26:23 jop.200821.a400 10 PROTON jop + + - + + + + jop_V_202_1 sref: reference peak not found default calibration done
24 12:51:27 fr.200821.a400 10 PROTON fr + + - + + + + FR-108-1E
18 11:49:05 jiz.200821.a400 20 PROTON jiz + + - - + + + JZ08_103_P1 sref: reference peak not found default calibration done
12 11:22:28 jiz.200821.a400 10 PROTON jiz + + - + + + + JZ08_103 sref: reference peak not found default calibration done
9 10:22:59 ial_35_1.200821.a400 10 PROTON ial + + - + + + +
7 09:37:50 jn312f8_23.200821.a400 11 C13 jn - + - - - + + jn312f8_23 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done; pp: Unable to assign a peak for scaling of E:/current_data/data/jn/nmr/jn312f8_23.200821.a400/11/pdata/1/peaks No peak is found in the specified ranges!
7 09:30:48 jn312f8_23.200821.a400 10 PROTON jn + + - + + + + jn312f8_23
23 02:15:26 ap.200820.a400 33 C13CPD ap - + - - - + + 7-9,11_F2 sref: reference peak not found default calibration done; pp: Unable to assign a peak for scaling of E:/current_data/data/ap/nmr/ap.200820.a400/33/pdata/1/peaks No peak is found in the specified ranges!
23 02:13:23 ap.200820.a400 32 P31CPD ap - + - - - + + 7-9,11_F2 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200820.a400/32/pdata/1/peaks!
23 02:04:09 ap.200820.a400 31 F19CPD_KU ap + + - + + + + 7-9,11_F2
5 22:04:45 cpo624.200820.a400 11 C13CPD cpo + + - + + + + CPO624 Purified sref: reference peak not found default calibration done
23 21:47:34 ap.200820.a400 30 PROTON ap + + - - + + + 7-9,11_F2
22 21:45:24 ap.200820.a400 22 P31CPD ap - + - - - + + 7-9,11_F1 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200820.a400/22/pdata/1/peaks!
22 21:43:04 ap.200820.a400 21 F19CPD_KU ap - + - - - + + 7-9,11_F1
22 21:25:26 ap.200820.a400 20 PROTON ap + + - + + + + 7-9,11_F1
24 21:23:17 ap.200820.a400 11 P31CPD ap - + - - - + + 7-9,11_F3
24 21:12:39 ap.200820.a400 10 PROTON ap + + - + + + + 7-9,11_F3 sref: reference peak not found default calibration done
20 20:52:29 at3_1_5.200820.a400 10 PROTON at - + - - - + +
20 20:32:09 at3_1_5.200820.a400 11 C13APT_KU at + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
4 19:24:07 gb.200820.a400 10 PROTON gb + + - + + + + GB-11-1crudeDMSO sref: reference peak not found default calibration done
14 19:01:31 yst.200820.a400 20 PROTON yst + + - - + + + YST-234 sref: reference peak not found default calibration done
13 18:54:11 yst.200820.a400 10 PROTON yst + + - + + + + YST-228
9 18:12:30 pd.200820.a400 41 P31CPD pd - + - - - + + PD-240-S2_2h
9 18:05:56 pd.200820.a400 40 PROTON pd + + - + + + + PD-240-S2_2h
6 17:53:21 pd.200820.a400 31 P31CPD pd - + - - - + + PD3-239CR_6h
6 17:45:40 pd.200820.a400 30 PROTON pd + + - + + + + PD3-239CR_6h
5 16:59:54 cpo624.200820.a400 10 PROTON cpo + + - + + + + CPO624 Purified sref: reference peak not found default calibration done
22 16:34:44 av.200820.a400 10 PROTON av + + - + + + + AV183 R 3rd fcc
21 16:28:31 pd.200820.a400 21 P31CPD pd - + - - - + + PD-240CR-S1
21 16:21:23 pd.200820.a400 20 PROTON pd + + - + + + + PD-240CR-S1
19 15:37:05 par.200820.a400 20 PROTON par + + - - x + + 102-003-cc topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
18 15:30:01 par.200820.a400 10 PROTON par + + - + + + + 102-002-pure
11 14:53:53 yd.200820.a400 30 C13 yd + + - + + + + YD-600-169-crude au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
9 14:51:41 pd.200820.a400 11 P31CPD pd - + - - - + + PD-239-CR_3h
9 14:43:51 pd.200820.a400 10 PROTON pd + + - + + + + PD-239-CR_3h
8 14:28:02 jn308f4_8.200820.a400 11 C13 jn - + - - - + + jn308f4_8 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 14:20:47 jn308f4_8.200820.a400 10 PROTON jn + + - + + + + jn308f4_8
10 14:10:53 cvh.200820.a400 10 PROTON cvh + + - + + + + CVI1-51 7-12 sref: reference peak not found default calibration done
5 13:23:31 fr.200820.a400 30 PROTON fr + + - + + + + FR-108-1C
1 12:47:45 yd.200820.a400 12 HSQC yd + + - + + + + YD-600-169-DMSO
2 12:31:59 yd.200820.a400 21 C13 yd - + - - - + + YD-600-169-CDCl3 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 12:24:56 yd.200820.a400 20 PROTON yd + + - + + + + YD-600-169-CDCl3
1 12:09:09 yd.200820.a400 11 C13 yd - + - - - + + YD-600-169-DMSO au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 12:02:30 yd.200820.a400 10 PROTON yd + + - + + + + YD-600-169-DMSO sref: reference peak not found default calibration done
22 11:46:44 fr.200820.a400 20 PROTON fr + + - + + + + FR-108-1B
23 11:08:22 fr.200820.a400 11 COSY fr - + - - - + + FR-108-1A - COSY
23 10:59:40 fr.200820.a400 10 PROTON fr + + - + + + + FR-108-1A - HNMR
24 09:58:30 asma.200820.a400 20 C13 asma + + - + + + + AM2-80-1 au_zg_max30min: --- au_zg_max30min finished ---
1 09:31:10 asma.200820.a400 10 PROTON asma + + - + + + + AM2-80-1 sref: reference peak not found default calibration done
18 23:55:26 at.200819.a400 13 COSY at - + - - - + +
18 23:04:44 at.200819.a400 12 HMBC_LP at + + - + + + +
24 22:00:36 ap.200819.a400 23 C13CPD ap + + - + + + + 7-15_F2 sref: reference peak not found default calibration done
14 19:21:13 gb.200819.a400 20 PROTON gb + + - + + + + GB-11-1-CRUDE sref: reference peak not found default calibration done
24 18:22:13 ap.200819.a400 22 HSQC ap - + - - - + + 7-15_F2
24 18:20:19 ap.200819.a400 21 P31CPD ap - + - - - + + 7-15_F2
24 18:09:44 ap.200819.a400 20 PROTON ap + + - - + + + 7-15_F2
23 18:07:49 ap.200819.a400 11 P31CPD ap - + - - - + + 7-15_F1
23 17:56:58 ap.200819.a400 10 PROTON ap + + - + + + + 7-15_F1
13 17:26:27 mci2e2rep2.200819.a400 10 PROTON mci + + - + + + +
19 16:51:04 pd.200819.a400 31 P31CPD pd - + - - - + + PD-237-S1_3h
19 16:43:40 pd.200819.a400 30 PROTON pd + + - + + + + PD-237-S1_3h
18 15:52:00 at.200819.a400 11 HSQC at - + - - - + +
18 15:45:09 at.200819.a400 10 PROTON at + + - + + + + sref: reference peak not found default calibration done
19 14:35:48 umb421_fr1.200819.a400 11 C13 umb + + - - + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
24 14:29:21 umb420fr2.200819.a400 10 PROTON umb + + - - + + +
23 14:21:58 umb420fr1.200819.a400 10 PROTON umb + + - - + + + sref: reference peak not found default calibration done
21 14:14:49 umb421fr3.200819.a400 10 PROTON umb + + - - + + +
20 14:08:14 umb421fr2.200819.a400 10 PROTON umb + + - - + + +
19 14:02:16 umb421_fr1.200819.a400 10 PROTON umb + + - - + + + sref: reference peak not found default calibration done
18 13:55:13 em36p2.200819.a400 10 PROTON emr + + - - + + + 1036p 15-21
17 13:48:11 em36p1.200819.a400 10 PROTON emr + + - - + + + 1036p 7-14
15 13:46:06 pd.200819.a400 21 P31CPD pd - + - - - + + PD-228-CR_15days
15 13:39:32 pd.200819.a400 20 PROTON pd + + - + + + + PD-228-CR_15days
13 13:22:25 av.200819.a400 20 PROTON av + + - + + + + AV1-83R
4 12:07:32 gb.200819.a400 10 PROTON gb + + - + + + + GB-10-5thspotboh2 sref: reference peak not found default calibration done
13 11:58:11 av.200819.a400 10 PROTON av + + - + + + + AV1-83
12 11:47:22 cvh.200819.a400 10 PROTON cvh + + - + + + + CVI1-39 lock: Command 'lock MeOD' failed. Lock is OFF
2 11:31:28 jiz.200819.a400 10 PROTON jiz + + - + + + + JZ08_101 sref: reference peak not found default calibration done
22 11:15:55 par.200819.a400 20 PROTON par + + - - + + + petasis reagent
24 11:08:56 par.200819.a400 10 PROTON par + + - + + + + new EtGly
14 10:54:11 mci2e2rep.200819.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
12 10:47:11 em1036c.200819.a400 10 PROTON emr + + - + + + +
11 10:40:37 ktt.200819.a400 10 PROTON ktt + + - + + + + KTT15-160_crude sref: reference peak not found default calibration done
9 10:24:18 pd.200819.a400 10 PROTON pd + + - + + + + PD-235-CR sref: reference peak not found default calibration done
8 10:16:11 ial_34_1b.200819.a400 10 PROTON ial + + - - + + +
7 10:08:03 ial_34_1a.200819.a400 10 PROTON ial + + - + + + +
5 09:16:11 fr.200819.a400 10 PROTON fr + + - + + + + 2-Br-4-cyclohexylphenyl starting material
11 19:47:19 gg.200818.a400 10 PROTON gg + + - + + + + GG01-69_Product sref: reference peak not found default calibration done
9 19:21:54 ap.200818.a400 31 P31CPD ap - + - - - + + 7-15_crude
9 19:11:02 ap.200818.a400 30 PROTON ap + + - + + + + 7-15_crude
22 18:29:35 jiz.200818.a400 10 PROTON jiz + + - + + + + JZ08_102 sref: reference peak not found default calibration done
20 17:07:41 yd.200818.a400 40 PROTON yd + + - - + + + YD-601-191-second spot sref: reference peak not found default calibration done
19 17:01:39 atcrystal.200818.a400 10 PROTON at + + - - + + + sref: reference peak not found default calibration done
18 16:55:03 atmastich.200818.a400 10 PROTON at + + - + + + + sref: reference peak not found default calibration done
17 16:40:06 kov.200818.a400 10 PROTON kov + + - + + + + KOV01-100 sref: reference peak not found default calibration done
8 16:31:23 fr.200818.a400 10 PROTON fr + + - + + + + FR-106-1A
12 16:21:57 yd.200818.a400 30 PROTON yd + + - + + + + YD- 3-dimethylamino- 1-propylamine sref: reference peak not found default calibration done
10 16:06:14 fm.200818.a400Fab35a 11 C13 fm - + - - - + + Fab35_after_hydrolysis CDCl3 13C 18/08/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 15:59:18 fm.200818.a400Fab35a 10 PROTON fm + + - + + + + Fab35_after_hydrolysis CDCl3 1H 18/08/20
5 15:49:49 cvh.200818.a400 20 PROTON cvh + + - + + + + CVI1-43 4-8
24 15:29:25 yd.200818.a400 20 C13 yd + + - + + + + YD-601-191-first spot au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
23 15:22:46 yd.200818.a400 10 PROTON yd + + - + + + + YD-601-191-second spot sref: reference peak not found default calibration done
22 15:15:16 av.200818.a400 20 PROTON av + + - + + + + AV1-83 StMat
21 15:08:27 av.200818.a400 10 PROTON av + + - + + + + AV1-71
20 14:47:40 umb417.200818.a400 10 PROTON umb + + - + + + + sref: reference peak not found default calibration done
8 13:39:40 cvh.200818.a400 10 PROTON cvh + + - + + + + CVI1-50 6-11
15 12:48:25 par.200818.a400 10 PROTON par + + - + + + + 103-001-crude
2 12:19:46 gb.200818.a400 20 PROTON gb + + - + + + + GB-10-4thspot
1 12:12:39 gb.200818.a400 10 PROTON gb + + - + + + + GB-10-5thboh sref: reference peak not found default calibration done
14 11:41:13 em.200818.a400 10 PROTON em + + - + + + + 147org_NH2_160%yield
8 11:02:51 mci2e2b.200818.a400 12 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 10:57:03 mci2e2b.200818.a400 11 COSY mci - + - - - + +
8 10:50:08 mci2e2b.200818.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
7 10:42:12 mci2e2a.200818.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
13 10:08:06 ial_34_1.200818.a400 10 PROTON ial + + - + + + +
11 09:37:49 ap.200818.a400 23 COSY ap - + - - - + + 7-12_2nd FCC_F
11 09:35:29 ap.200818.a400 22 F19CPD_KU ap - + - - - + + 7-12_2nd FCC_F
11 09:33:34 ap.200818.a400 21 P31CPD ap - + - - - + + 7-12_2nd FCC_F
11 09:21:57 ap.200818.a400 20 PROTON ap + + - + + + + 7-12_2nd FCC_F
9 09:14:59 ap.200818.a400 10 P31CPD ap + + - + + + + pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200818.a400/10/pdata/1/peaks!
5 00:25:45 jn307f9_14.200817.a400 22 HSQC jn - + - - - + + jn307f9_14
5 23:20:27 jn307f9_14.200817.a400 21 C13CPD jn + + - + + + + jn307f9_14 sref: reference peak not found default calibration done
16 23:20:02 em.200817.a400 42 COSY em - + - - - x - 116abf-20-24-32 au_getlcosy: Can't get CURDATA2 parameters., Acquisition Failed
16 23:04:37 em.200817.a400 43 HSQC em - + - - - + + 116abf-20-24-32
16 22:00:26 em.200817.a400 41 C13CPD em + + - + + + + 116abf-20-24-32 sref: reference peak not found default calibration done
5 21:19:07 jn307f9_14.200817.a400 20 PROTON jn + + - - + + + jn307f9_14
4 21:03:25 fm.200817.a400Fab35m 21 C13 fm - + - - - + + Fab35_merda_bis CDCl3| 13C 17/08/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
4 20:55:45 fm.200817.a400Fab35m 20 PROTON fm + + - - + + + Fab35_merda_bis CDCl3| 1H 17/08/20
23 20:50:45 gb.200817.a400 40 PROTON gb + + - - x + + GB-10-5thspot topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
15 20:43:54 gb.200817.a400 30 PROTON gb + + - - + + + GB-10-4thspot sref: reference peak not found default calibration done
10 20:13:50 mci2e1b.200817.a400 12 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 20:08:01 mci2e1b.200817.a400 11 COSY mci - + - - - + +
10 20:01:19 mci2e1b.200817.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
1 19:52:50 mci2e1a.200817.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
14 19:45:56 gb.200817.a400 20 PROTON gb + + - - + + + GB-1-1stspot sref: reference peak not found default calibration done
13 19:37:56 gb.200817.a400 10 PROTON gb + + - + + + + GB-9-CRUDE sref: reference peak not found default calibration done
3 19:29:28 av.200817.a400 10 PROTON av + + - + + + + AV1-83
2 19:13:30 fm.200817.a400Fab35m 11 C13 fm - + - - - + + Fab35_merda CDCl3 13C 17/08/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 19:06:19 fm.200817.a400Fab35m 10 PROTON fm + + - - + + + Fab35_merda CDCl3 1H 17/08/20
21 18:58:12 cbc.200817.a400 30 PROTON cbc + + - - + + + 23s2
20 18:49:36 cbc.200817.a400 20 PROTON cbc + + - - + + + 23b2
19 18:40:27 cbc.200817.a400 10 PROTON cbc + + - + + + + 23b1
24 18:23:39 cpo624.200817.a400 20 PROTON cpo + + - + + + + sref: reference peak not found default calibration done
5 18:15:44 jn307f9_14.200817.a400 10 PROTON jn + + - + + + + jn307 f9_14
7 18:13:37 ap.200817.a400 51 P31CPD ap - + - - - + + 7-14_F3
7 18:02:40 ap.200817.a400 50 PROTON ap + + - - + + + 7-14_F3
8 17:51:44 ap.200817.a400 40 PROTON ap + + - + + + + 7-14_F3 sref: reference peak not found default calibration done
12 17:21:43 cpo624.200817.a400 11 C13 cpo - + - - - + + CPO624-C au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
12 17:14:33 cpo624.200817.a400 10 PROTON cpo + + - + + + + CPO624-C
9 16:26:36 ap.200817.a400 32 HSQC ap - + - - - + + 7-14_F2
9 16:24:41 ap.200817.a400 31 P31CPD ap - + - - - + + 7-14_F2
9 16:13:37 ap.200817.a400 30 PROTON ap + + - + + + + 7-14_F2 sref: reference peak not found default calibration done
6 15:47:15 cvh.200817.a400 50 PROTON cvh + + - + + + + CVI1-49 4-10
22 15:35:21 gg.200817.a400 10 PROTON gg + + - + + + + GG01-71_Product sref: reference peak not found default calibration done
8 15:33:25 ap.200817.a400 21 P31CPD ap - + - - - + + 7-14_F0
8 15:25:08 ap.200817.a400 20 PROTON ap + + - + + + + 7-14_F0
7 15:22:55 ap.200817.a400 11 P31CPD ap - + - - - + + 7-14_F3
7 15:11:29 ap.200817.a400 10 PROTON ap + + - + + + + 7-14_F3 sref: reference peak not found default calibration done
16 14:54:58 em.200817.a400 40 PROTON em + + - + + + + 116abf-20-24-32 sref: reference peak not found default calibration done
18 14:48:42 em.200817.a400 60 PROTON em + + - - x + + 146he_f1 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
17 14:39:36 em.200817.a400 50 PROTON em + + - - + + + 146he_f24
10 14:23:50 fm.200817.a400Fab34b 11 C13 fm - + - - - + + Fab34_crude_bis CDCl3 13C 17/08/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 14:16:05 fm.200817.a400Fab34b 10 PROTON fm + + - - + + + Fab34_crude_bis CDCl3 1H 17/08/20
2 14:10:16 cyl.200817.a400 12 COSY cyl - + - - - + + MCD_CL-02-38
2 13:54:29 cyl.200817.a400 11 C13 cyl - + - - - + + MCD_CL-02-38 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 13:48:12 cyl.200817.a400 10 PROTON cyl + + - + + + + MCD_CL-02-38 sref: reference peak not found default calibration done
20 13:23:58 jiz.200817.a400 20 PROTON jiz + + - - + + + JZ08_96_solid cake sref: reference peak not found default calibration done
19 13:07:58 jiz.200817.a400 10 PROTON jiz + + - + + + + JZ08_89 sref: reference peak not found default calibration done
15 12:25:35 em.200817.a400 30 PROTON em + + - - + + + 146he_I_CLoxalate
14 12:14:55 em.200817.a400 21 PROTON em + + - - + + + 146he_f2 tms-oxalate
13 12:04:15 em.200817.a400 11 PROTON em + + - + + + + 146he_f17 tms-oxalate
7 11:47:08 cvh.200817.a400 40 PROTON cvh + + - - + + + CVI1-39 9-15
11 11:17:05 mci95.200817.a400 12 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 11:11:16 mci95.200817.a400 11 COSY mci - + - - - + +
11 11:03:27 mci95.200817.a400 10 PROTON mci + + - - + + +
14 10:52:48 em.200817.a400 20 PROTON em + + - - + + + 146he_f11 tms-oxalate
13 10:42:09 em.200817.a400 10 PROTON em + + - - + + + 146he_f20 tms-oxalate
8 10:34:51 cvh.200817.a400 30 PROTON cvh + + - - + + + CVI1-49 4-10
9 10:29:30 cvh.200817.a400 20 PROTON cvh + + - - x + + CVI1-46 14-22 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
10 10:22:02 cvh.200817.a400 10 PROTON cvh + + - - + + + CVI1-43 4-8
1 10:06:19 fm.200817.a400Fab34c 11 C13 fm - + - - - + + Fab34_crude CDCl3 13C 17/08/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 09:59:02 fm.200817.a400Fab34c 10 PROTON fm + + - + + + + Fab34_crude CDCl3 1H 17/08/20
20 22:00:21 ap.200816.a400 93 C13CPD ap + + - + + + + 7-12_2nd FCC_F3 sref: reference peak not found default calibration done
23 20:41:50 jiz.200816.a400 20 PROTON jiz + + - + + + + JZ08_99 sref: reference peak not found default calibration done
20 20:13:51 ap.200816.a400 92 HSQC ap + + - - + + + 7-12_2nd FCC_F3
8 20:11:30 ap.200816.a400 131 F19CPD_KU ap - + - - - + + 7-13 (newest S-MTPA rxn test)
8 20:04:05 ap.200816.a400 130 PROTON ap + + - + + + + 7-13 (newest S-MTPA rxn test)
17 20:02:00 ap.200816.a400 121 P31CPD ap - + - - - + + 7-14 (newest LPC palmitate)
17 19:51:12 ap.200816.a400 120 PROTON ap + + - + + + + 7-14 (newest LPC palmitate)
9 19:48:58 ap.200816.a400 111 F19CPD_KU ap - + - - - + + 7-11
9 19:37:20 ap.200816.a400 110 PROTON ap + + - - + + + 7-11
20 19:35:24 ap.200816.a400 91 P31CPD ap - + - - - + + 7-12_2nd FCC_F3
20 19:23:19 ap.200816.a400 90 PROTON ap + + - - + + + 7-12_2nd FCC_F3 sref: reference peak not found default calibration done
21 19:21:24 ap.200816.a400 81 P31CPD ap - + - - - + + 7-12_2nd FCC_F4
21 19:09:41 ap.200816.a400 80 PROTON ap + + - - + + + 7-12_2nd FCC_F4
1 19:03:07 ap.200816.a400 70 PROTON ap + + - - + + + CDCl3 sref: reference peak not found default calibration done
24 19:01:07 ap.200816.a400 61 P31CPD ap - + - - - + + 7-12_2nd FCC_F2
24 18:49:01 ap.200816.a400 60 PROTON ap + + - - + + + 7-12_2nd FCC_F2
23 18:46:56 ap.200816.a400 51 P31CPD ap - + - - - + + 7-12_2nd FCC_F1
23 18:35:58 ap.200816.a400 50 PROTON ap + + - + + + + 7-12_2nd FCC_F1 sref: reference peak not found default calibration done
10 16:10:17 ktt.200816.a400 10 PROTON ktt + + - + + + + KTT15-146_pur sref: reference peak not found default calibration done
7 04:13:43 ap.200816.a400 42 F19CPD_KU ap - + - - - + + 7-12_F2 (f62,65-73,76-82)
7 04:11:35 ap.200816.a400 41 P31CPD ap - + - - - + + 7-12_F2 (f62,65-73,76-82)
7 03:57:46 ap.200816.a400 40 PROTON ap + + - - + + + 7-12_F2 (f62,65-73,76-82)
8 03:55:31 ap.200816.a400 32 F19CPD_KU ap - + - - - + + 7-12_F4
8 03:53:24 ap.200816.a400 31 P31CPD ap - + - - - + + 7-12_F4
8 03:40:34 ap.200816.a400 30 PROTON ap + + - - + + + 7-12_F4 sref: reference peak not found default calibration done
21 03:38:16 ap.200816.a400 22 F19CPD_KU ap - + - - - + + 7-12_F1 (f57-61)
21 03:35:57 ap.200816.a400 21 P31CPD ap - + - - - + + 7-12_F1 (f57-61)
21 03:22:53 ap.200816.a400 20 PROTON ap + + - - + + + 7-12_F1 (f57-61)
20 02:22:53 ap.200816.a400 14 C13CPD ap - + - - - + + 7-12_F3 (f63,64) sref: reference peak not found default calibration done
20 02:07:08 ap.200816.a400 13 HSQC ap - + - - - + + 7-12_F3 (f63,64)
20 02:04:50 ap.200816.a400 12 F19CPD_KU ap - + - - - + + 7-12_F3 (f63,64)
20 02:02:45 ap.200816.a400 11 P31CPD ap - + - - - + + 7-12_F3 (f63,64)
20 01:51:40 ap.200816.a400 10 PROTON ap + + - + + + + 7-12_F3 (f63,64) sref: reference peak not found default calibration done
8 17:35:18 ap.200815.a400 31 F19CPD_KU ap - + - - - + + (S)-MTPA
8 17:23:59 ap.200815.a400 30 PROTON ap + + - + + + + (S)-MTPA
17 15:12:46 ap.200815.a400 23 HSQC ap + + - - + + + 7-10_F1
20 14:53:13 ap.200815.a400 13 HSQC ap + + - - + + + 7-10_prep HPLC_F2
17 14:50:58 ap.200815.a400 22 F19CPD_KU ap - + - - - + + 7-10_F1
17 14:48:52 ap.200815.a400 21 P31CPD ap - + - - - + + 7-10_F1
17 14:37:45 ap.200815.a400 20 PROTON ap + + - - + + + 7-10_F1 sref: reference peak not found default calibration done
20 14:35:26 ap.200815.a400 12 F19CPD_KU ap - + - - - + + 7-10_prep HPLC_F2
20 14:33:31 ap.200815.a400 11 P31CPD ap - + - - - + + 7-10_prep HPLC_F2
20 14:22:40 ap.200815.a400 10 PROTON ap + + - + + + + 7-10_prep HPLC_F2 sref: reference peak not found default calibration done
7 00:05:45 ap.200814.a400 21 P31CPD ap - + - - - + + 7-8_crude
7 23:50:15 ap.200814.a400 22 HSQC ap - + - - - + + 7-8_crude
7 23:39:34 ap.200814.a400 20 PROTON ap + + - + + + + 7-8_crude
22 19:50:20 mci94.200814.a400 12 COSY mci - + - - - + +
22 19:19:59 mci94.200814.a400 11 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
22 19:13:14 mci94.200814.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
19 18:52:10 yd.200814.a400 10 PROTON yd + + - + + + + YD-601-191-pure
18 18:34:08 gg.200814.a400 40 PROTON gg + + - - + + + GG01-57_Product sref: reference peak not found default calibration done
14 18:27:43 fba.200814.a400 40 PROTON fba + + - + + + + FB-L-NIP-D sref: reference peak not found default calibration done
13 18:20:42 fba.200814.a400 30 PROTON fba + + - + + + + FB-L-NIP-W sref: reference peak not found default calibration done
12 18:13:50 fba.200814.a400 20 PROTON fba + + - + + + + FB-D-NIP-D sref: reference peak not found default calibration done
11 18:06:58 fba.200814.a400 10 PROTON fba + + - + + + + FB-D-NIP-W sref: reference peak not found default calibration done
3 15:32:48 jiz.200814.a400 10 PROTON jiz + + - + + + + JZ08_94 sref: reference peak not found default calibration done
24 15:08:56 ap.200814.a400 12 F19CPD_KU ap + + - + + + + 7-9_crude
5 14:34:53 par.200814.a400 20 PROTON par + + - - x + + 104-001-test-reagent topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
4 14:27:55 par.200814.a400 10 PROTON par + + - + + + + 103-001-second pure
24 14:21:26 ap.200814.a400 11 P31CPD ap - + - - - + + 7-9_crude
24 14:10:25 ap.200814.a400 10 PROTON ap + + - + + + + 7-9_crude
14 14:07:59 fr.200814.a400 21 F19CPD_KU fr - + - - - + + FR-105-1B F19 WITH DECOUPLING
14 14:01:25 fr.200814.a400 20 PROTON fr + + - + + + + FR-105-1B - HNMR
8 12:55:51 cv.200814.a400 40 PROTON cv + + - - + + + 95/50 UV sref: reference peak not found default calibration done
7 12:38:41 cv.200814.a400 30 PROTON cv + + - - + + + 95/5 UV sref: reference peak not found default calibration done
10 12:31:52 mci93b.200814.a400 10 PROTON mci + + - - + + +
9 12:26:04 mci93a.200814.a400 12 COSY mci - + - - - + +
9 12:23:47 mci93a.200814.a400 11 PROTON mci - + - - - + + sref: reference peak not found default calibration done
9 11:47:52 mci93a.200814.a400 10 C13 mci + + - - + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
6 11:31:38 cv.200814.a400 20 PROTON cv + + - + + + + 95/50 Autoclave sref: reference peak not found default calibration done
5 11:15:23 cv.200814.a400 10 PROTON cv + + - + + + + 95/5 Autoclave sref: reference peak not found default calibration done
3 10:24:24 gg.200814.a400 30 PROTON gg + + - - x + + GG01-63_P topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
2 10:17:27 gg.200814.a400 20 PROTON gg + + - - + + + GG01-61_P
1 10:10:17 gg.200814.a400 10 PROTON gg + + - - + + + GG01-59_P
14 10:04:33 fr.200814.a400 11 COSY fr - + - - - + + FR-105-1A - COSY
14 09:56:19 fr.200814.a400 10 PROTON fr + + - + + + + FR-105-1A - HNMR
9 23:16:33 ap.200813.a400 12 F19CPD_KU ap - + - - - + + 7-10
9 23:14:20 ap.200813.a400 11 P31CPD ap - + - - - + + 7-10
9 23:03:01 ap.200813.a400 10 PROTON ap + + - + + + + 7-10_crude
22 20:11:58 ktt.200813.a400 10 PROTON ktt + + - + + + + KTT15-138_pur sref: reference peak not found default calibration done
19 19:03:18 cv.200813.a400 100 PROTON cv + + - - + + + CV051 CsH sref: reference peak not found default calibration done
18 18:46:10 cv.200813.a400 90 PROTON cv + + - - + + + CV051 F1 Batch 3/4 supernatant sref: reference peak not found default calibration done
17 18:29:24 cv.200813.a400 80 PROTON cv + + - - + + + CV051 F1 Batch 1/2 supernatant sref: reference peak not found default calibration done
16 18:13:58 cv.200813.a400 70 PROTON cv + + - - + + + LA 110 Su 55 2M 37C rga: This RG value has already been tried before, therefore RG is now fixed to 114.00., sref: reference peak not found default calibration done
15 17:58:17 cv.200813.a400 60 PROTON cv + + - - + + + LA 110 Su 55 2M RT sref: reference peak not found default calibration done
14 17:41:42 cv.200813.a400 50 PROTON cv + + - + + + + LA 110 Su 55 2M 4C sref: reference peak not found default calibration done
20 17:33:59 mci93a.200813.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
13 17:17:32 cv.200813.a400 40 PROTON cv + + - - + + + LA 32.5 2M 37C sref: reference peak not found default calibration done
12 17:01:12 cv.200813.a400 30 PROTON cv + + - + + + + LA 32.5 2M RT sref: reference peak not found default calibration done
7 16:45:12 av.200813.a400 21 C13 av - + - - - + + AV1-82 wp au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
7 16:37:15 av.200813.a400 20 PROTON av + + - + + + + AV1-82 wp
11 16:21:55 cv.200813.a400 20 PROTON cv + + - - + + + LA 32.5 2M 4C sref: reference peak not found default calibration done
10 16:05:56 cv.200813.a400 10 PROTON cv + + - + + + + CV063 95/50 Atto665 bis sref: reference peak not found default calibration done
6 15:22:21 kov.200813.a400 10 PROTON kov + + - + + + + KOV01-94
10 14:15:29 cvh.200813.a400 11 PROTON cvh + + - + + + + CVI1-47 prep
2 14:08:51 cyl.200813.a400 10 PROTON cyl + + - + + + + MCD_CL-02-42 sref: reference peak not found default calibration done
10 13:32:52 cvh.200813.a400 10 PROTON cvh + + - + + + + CVI1-47 prep
15 13:24:04 stja.200813.a400 10 PROTON stja + + - + + + + 62 HYDRAZON
13 13:16:20 av.200813.a400 10 PROTON av + + - + + + + AV1-82
3 12:09:53 gb.200813.a400 20 PROTON gb + + - - + + + GB-7-2-CONTROL sref: reference peak not found default calibration done
4 12:02:23 gb.200813.a400 10 PROTON gb + + - + + + + GB-9-1-CRUDE sref: reference peak not found default calibration done
11 11:13:05 fr.200813.a400 12 F19CPD_KU fr - + - - - + + FR-104-1B F19 WITH DECOUPLING
11 11:07:19 fr.200813.a400 11 COSY fr - + - - - + + FR-104-1B COSY
11 10:59:56 fr.200813.a400 10 PROTON fr + + - + + + + FR-104-1B HNMR
5 10:43:01 mci93f3387.200813.a400 11 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 10:37:55 mci93f3387.200813.a400 10 PROTON mci + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, Lock anomaly during acquisition, sref: reference peak not found default calibration done
1 10:29:51 ed.200813.a400 10 PROTON ed + + - + + + + Emil, bromering, biprodukt
19 10:03:27 at5_4_3.200813.a400 10 PROTON at + + - + + + +
17 22:20:33 ap.200812.a400 13 C13CPD ap - + - - - + + 7-7 sref: reference peak not found default calibration done
17 22:04:53 ap.200812.a400 12 HSQC ap - + - - - + + 7-7
17 22:02:38 ap.200812.a400 11 P31CPD ap - + - - - + + 7-7
17 21:51:58 ap.200812.a400 10 PROTON ap + + - + + + + 7-7
4 21:42:31 mci90f513.200812.a400 10 PROTON mci + + - + + + +
20 16:21:44 gg.200812.a400 10 PROTON gg + + - + + + + GG01-55_Organic layer sref: reference peak not found default calibration done
12 15:29:58 ial_29_1.200812.a400 20 PROTON ial + + - + + + +
18 15:22:07 fr.200812.a400 10 PROTON fr + + - + + + + 4-Br-Acephenone
8 14:35:56 ial_29_1.200812.a400 10 PROTON ial + + - + + + +
16 13:26:51 jiz.200812.a400 20 PROTON jiz + + - - + + + JZ08_86 sref: reference peak not found default calibration done
14 13:11:06 jiz.200812.a400 10 PROTON jiz + + - - + + + JZ08_84 sref: reference peak not found default calibration done
11 13:05:05 yd.200812.a400 10 PROTON yd + + - + + + + YD-510-190-pure sref: reference peak not found default calibration done
10 12:07:28 cvh.200812.a400 20 PROTON cvh + + - + + + + CVI1-47 11-13
5 12:01:40 jop.200812.a400 12 COSY jop - + - - - + + jop_v_200_1
5 11:31:43 jop.200812.a400 11 C13 jop - + - - - + + jop_v_200_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 11:24:30 jop.200812.a400 10 PROTON jop + + - + + + + jop_v_200_1 sref: reference peak not found default calibration done
11 11:03:56 asma.200812.a400 10 C13 asma + + - + + + + AM2-79-3 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
5 09:14:22 cvh.200812.a400 10 PROTON cvh + + - + + + + CVI1-48 5-9
14 00:59:43 par.200811.a400 20 PROTON par + + - - x + + 103-001-bp topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
15 00:52:44 par.200811.a400 10 PROTON par + + - - + + + 103-001-pure
13 00:23:15 em.200811.a400 13 HSQC em - + - - - + + 146wu
13 00:02:57 em.200811.a400 12 COSY em - + - - - + + 146wu
13 22:00:10 em.200811.a400 11 C13CPD em + + - + + + + 146wu sref: reference peak not found default calibration done
10 20:20:13 gg.200811.a400 20 PROTON gg + + - + + + + GG01-42_48_Product
19 18:56:05 mci.200811.a400 20 PROTON mci + + - - + + + mc90 B sref: reference peak not found default calibration done
18 18:48:46 mci.200811.a400 10 PROTON mci + + - + + + + mc90 A sref: reference peak not found default calibration done
13 17:32:48 em.200811.a400 10 PROTON em + + - + + + + 146wu
11 15:57:57 ap.200811.a400 11 P31CPD ap - + - - - + + 7-7_crude
11 15:47:28 ap.200811.a400 10 PROTON ap + + - + + + + 7-7_crude
1 14:48:17 fm.200811.a400Fab30 11 C13 fm - + - - - + + Fab30 after hydrolysis CDCl3 13C 11/08/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 14:40:53 fm.200811.a400Fab30 10 PROTON fm + + - + + + + Fab30 after hydrolysis CDCl3 1H 11/08/20
10 14:00:08 gg.200811.a400 10 PROTON gg + + - - x + + GG01-51_53_Product topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
6 13:52:45 fr.200811.a400 20 PROTON fr + + - + + + + 4-CF3-phenylboronic acid
16 13:43:20 ktt.200811.a400 20 PROTON ktt + + - + + + + KTT15-114_recov
12 12:16:15 cvh.200811.a400 10 PROTON cvh + + - + + + + cvi1-43 4-8
8 11:34:00 ktt.200811.a400 10 PROTON ktt + + - + + + + KTT15-116_crude sref: reference peak not found default calibration done
5 09:59:18 fr.200811.a400 11 COSY fr - + - - - + + FR-103-1A - COSY
5 09:50:49 fr.200811.a400 10 PROTON fr + + - + + + + FR-103-1A
15 22:06:09 ap.200810.a400 13 C13CPD ap + + - + + + + 7-6 sref: reference peak not found default calibration done
7 21:59:02 par.200810.a400 50 PROTON par + + - + + + + 103-002-crudecrude
1 20:26:29 mci92f5682.200810.a400 20 PROTON mci + + - + + + + sref: reference peak not found default calibration done
9 19:31:48 av.200810.a400 11 C13 av + + - + + + + AV1-81 8-13 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
9 19:16:59 av.200810.a400 10 PROTON av + + - + + + + AV1-81 8-13
15 19:01:18 ap.200810.a400 11 HSQC ap - + - - - + + 7-6
15 18:59:15 ap.200810.a400 12 P31CPD ap - + - - - + + 7-6
15 18:48:13 ap.200810.a400 10 PROTON ap + + - + + + + 7-6
8 18:05:31 par.200810.a400 90 PROTON par + + - - + + + ETOAC
3 18:00:37 par.200810.a400 80 PROTON par + + - - x + + DCM topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
1 17:53:53 par.200810.a400 70 PROTON par + + - - + + + cdcl3-new
23 17:50:32 ph.200810.a400 42 F19CPD_KU ph - + - - - + + 6-difluoromethylnicotine crude
23 17:35:33 ph.200810.a400 40 PROTON ph + + - - x + + 6-difluoromethylnicotine crude topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
2 17:27:43 par.200810.a400 60 PROTON par + + - - + + + heptane
22 16:52:45 ph.200810.a400 31 C13 ph + + - - + + + 6-aminonicotine (and 2-aminonicotine) au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
21 16:18:00 ph.200810.a400 21 C13 ph + + - - + + + 6-bromonicotine purified au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
19 16:11:12 par.200810.a400 41 PROTON par + + - - + + + 103-001-after filter on wattm
17 16:03:53 par.200810.a400 21 PROTON par + + - - + + + 100-004-a-crude
22 15:56:04 ph.200810.a400 30 PROTON ph + + - - + + + 6-aminonicotine (and 2-aminonicotine)
21 15:47:39 ph.200810.a400 20 PROTON ph + + - - + + + 6-bromonicotine purified
20 15:17:20 ph.200810.a400 11 C13 ph - + - - - + + Methylnicotine (and nicotine) au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
20 15:08:48 ph.200810.a400 10 PROTON ph + + - + + + + Methylnicotine (and nicotine)
9 14:34:39 cvh.200810.a400 10 PROTON cvh + + - + + + + cvi1-43 4-8
19 13:59:55 par.200810.a400 40 PROTON par + + - - x + + 103-001-after filter on wattm topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
18 13:53:18 par.200810.a400 30 PROTON par + + - - + + + 100-008-a-crude
17 13:48:33 par.200810.a400 20 PROTON par + + - - x + + 100-004-a-crude topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
16 13:31:52 par.200810.a400 10 PROTON par + + - + + + + 103-001-crudecrude
13 11:49:59 hl.200810.a400 42 P31CPD hl - + - - - + + DAD_040_F 24.
13 11:34:12 hl.200810.a400 41 C13 hl - + - - - + + DAD_040_F 24. au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
13 11:27:49 hl.200810.a400 40 PROTON hl + + - - + + + DAD_040_F 24.
12 11:25:40 hl.200810.a400 32 P31CPD hl - + - - - + + DAD_040_F 19. pp: Cannot find any peak for scaling in E:/current_data/data/hl/nmr/hl.200810.a400/32/pdata/1/peaks!
12 11:09:42 hl.200810.a400 31 C13 hl - + - - - + + DAD_040_F 19. au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
12 11:03:26 hl.200810.a400 30 PROTON hl + + - - + + + DAD_040_F 19.
11 11:01:12 hl.200810.a400 22 P31CPD hl - + - - - + + DAD_040_F 16
11 10:45:26 hl.200810.a400 21 C13 hl - + - - - + + DAD_040_F 16 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 10:38:56 hl.200810.a400 20 PROTON hl + + - - + + + DAD_040_F 16 sref: reference peak not found default calibration done
10 10:36:42 hl.200810.a400 12 P31CPD hl - + - - - + + DAD_040_F 11.
10 10:20:55 hl.200810.a400 11 C13 hl - + - - - + + DAD_040_F 11. au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
10 10:14:14 hl.200810.a400 10 PROTON hl + + - + + + + DAD_040_F 11.
7 10:07:10 mci92f99104.200810.a400 10 PROTON mci + + - - + + +
6 09:51:28 mci92f5682.200810.a400 11 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
6 09:46:41 mci92f5682.200810.a400 10 PROTON mci + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
5 09:39:06 mci92f3449.200810.a400 10 PROTON mci + + - - + + +
4 09:32:00 mci92f2233.200810.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
3 10:02:27 par.200809.a400 30 PROTON par + + - - + + + cdcl3-ds
2 09:55:44 par.200809.a400 20 PROTON par + + - - + + + Et3N
1 09:48:43 par.200809.a400 10 PROTON par + + - + + + + DMAP
17 15:09:53 mci91f1921.200808.a400 10 PROTON mci + + - - + + + sref: reference peak not found default calibration done
16 15:04:04 mci91f2259.200808.a400 12 COSY mci - + - - - + +
16 14:48:22 mci91f2259.200808.a400 11 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
16 14:41:27 mci91f2259.200808.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
12 14:08:03 gg.200808.a400 10 PROTON gg + + - + + + + GG01-50S sref: reference peak not found default calibration done
10 02:31:33 em.200807.a400 13 HSQC em - + - - - + + 144sm
10 02:11:24 em.200807.a400 12 COSY em - + - - - + + 144sm
10 01:11:29 em.200807.a400 11 C13CPD em - + - - - + + 144sm sref: reference peak not found default calibration done
10 00:54:13 em.200807.a400 10 PROTON em + + - + + + + 144sm
19 00:44:01 ap.200807.a400 40 PROTON ap + + - - + + + 7-5_F3 (f50-53)
18 00:33:42 ap.200807.a400 30 PROTON ap + + - - + + + 7-5_F2 (f49) sref: reference peak not found default calibration done
17 23:34:00 ap.200807.a400 22 C13CPD ap - + - - - + + 7-5_F1 (f43-48) sref: reference peak not found default calibration done
17 23:18:18 ap.200807.a400 21 HSQC ap - + - - - + + 7-5_F1 (f43-48)
17 23:07:06 ap.200807.a400 20 PROTON ap + + - + + + + 7-5_F1 (f43-48)
12 23:04:41 ial_33_1.200807.a400 12 F19CPD_KU ial - + - - - + +
12 22:00:16 ial_33_1.200807.a400 11 C13CPD ial + + - + + + + sref: reference peak not found default calibration done
13 21:25:17 yd.200807.a400 40 PROTON yd + + - + + + + YD-607-186-WASHED WITH ETHER sref: reference peak not found default calibration done
18 20:36:15 av.200807.a400 10 PROTON av + + - + + + + AV1-80
14 20:05:05 yd.200807.a400 30 PROTON yd + + - - + + + YD-508-185-starting material after column sref: reference peak not found default calibration done
13 19:58:05 yd.200807.a400 20 PROTON yd + + - + + + + YD-508-185-pure
6 18:52:07 yd.200807.a400 10 PROTON yd + + - - + + + YD-512-187-crude
5 18:49:54 pd.200807.a400 21 F19CPD_KU pd - + - - - + + PD-234A
5 18:43:03 pd.200807.a400 20 PROTON pd + + - + + + + PD-234A
4 18:40:44 pd.200807.a400 11 F19CPD_KU pd - + - - - + + PD-234B
4 18:34:08 pd.200807.a400 10 PROTON pd + + - + + + + PD-234B
3 18:27:35 jiz.200807.a400 20 PROTON jiz + + - - + + + JZ08_62_impurity
2 18:20:39 jiz.200807.a400 10 PROTON jiz + + - + + + + JZ08_70
12 18:12:43 ial_33_1.200807.a400 10 PROTON ial + + - - + + + sref: reference peak not found default calibration done
20 18:06:26 ktt.200807.a400 30 PROTON ktt + + - + + + + KTT15-106_crude sref: reference peak not found default calibration done
19 17:38:43 at5_9_3.200807.a400 10 PROTON at + + - - + + +
17 17:36:15 jop.200807.a400 22 P31 jop - + - - - + + DAD043 P2
17 17:20:20 jop.200807.a400 21 C13 jop - + - - - + + DAD043 P2 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
17 17:13:18 jop.200807.a400 20 PROTON jop + + - - + + + DAD043 P2
16 17:10:45 jop.200807.a400 12 P31 jop - + - - - + + DAD043 P1
16 16:55:03 jop.200807.a400 11 C13 jop - + - - - + + DAD043 P1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
16 16:47:42 jop.200807.a400 10 PROTON jop + + - + + + + DAD043 P1
1 16:27:58 ed.200807.a400 10 PROTON ed + + - + + + + emil - ester intermediat, 2. vask
13 16:17:13 ap.200807.a400 10 PROTON ap + + - + + + + NYR-4
19 15:30:10 fr.200807.a400 40 PROTON fr + + - + + + + FR-102-1E
15 13:52:46 fr.200807.a400 30 PROTON fr + + - + + + + FR-102-1C
11 12:57:22 ktt.200807.a400 20 PROTON ktt + + - + + + + KTT15-110_pur
8 11:51:51 ktt.200807.a400 11 COSY ktt - + - - - + + KTT15-108_pur
8 11:45:09 ktt.200807.a400 10 PROTON ktt + + - + + + + KTT15-108_pur sref: reference peak not found default calibration done
7 11:36:57 fr.200807.a400 20 PROTON fr + + - - + + + FR-102-1B -MORE CONCENTRATED
5 11:15:43 mci89.200807.a400 11 HSQC mci + + - + + + +
21 11:07:58 par.200807.a400 50 PROTON par + + - + + + + VINCE LACTAM-DMSO sref: reference peak not found default calibration done
2 11:02:15 fr.200807.a400 11 COSY fr - + - - - + +
2 10:57:01 fr.200807.a400 10 PROTON fr + + - - x + + FR-102-1B topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
9 10:49:18 par.200807.a400 40 PROTON par + + - - + + + JUST SOLVENT
10 10:41:44 cvh.200807.a400 10 PROTON cvh + + - - + + + CVI1-43 4-8
5 10:34:07 mci89.200807.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
24 10:01:24 par.200807.a400 30 PROTON par + + - - + + + o(t-buo)2
23 09:56:13 par.200807.a400 20 PROTON par + + - - x + + vince lactam-other one topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
22 09:47:25 par.200807.a400 10 PROTON par + + - + + + + 31813-vince lactam
5 22:00:10 ki513_2ny.200806.a400 11 C13CPD ki + + - + + + + KI 513-2 sref: reference peak not found default calibration done
15 20:19:51 yd.200806.a400 21 PROTON yd - + - - - + + YD-607-179-crude sref: reference peak not found default calibration done
15 19:51:58 yd.200806.a400 20 PROTON yd + + - + + + + YD-607-179-crude sref: reference peak not found default calibration done
16 19:46:14 cbc.200806.a400 11 COSY cbc - + - - - + + CBC137 crude
16 19:39:11 cbc.200806.a400 10 PROTON cbc + + - + + + + CBC137 crude
13 19:22:40 cv.200806.a400 80 PROTON cv + + - + + + + 95/5 1M 4C sref: reference peak not found default calibration done
18 19:15:30 av.200806.a400 30 PROTON av + + - - + + + AV1-79 33
17 19:08:24 av.200806.a400 20 PROTON av + + - + + + + AV1-79 22 31
12 18:52:35 cv.200806.a400 70 PROTON cv + + - - + + + 95/5 1M RT sref: reference peak not found default calibration done
11 18:36:36 cv.200806.a400 60 PROTON cv + + - - + + + 95/5 1M 37C sref: reference peak not found default calibration done
10 18:20:58 cv.200806.a400 50 PROTON cv + + - - + + + 95/50 1M 4C sref: reference peak not found default calibration done
9 18:04:14 cv.200806.a400 40 PROTON cv + + - + + + + 95/50 1M RT sref: reference peak not found default calibration done
14 17:56:28 yd.200806.a400 10 PROTON yd + + - + + + + YD-606-178
8 17:40:59 cv.200806.a400 30 PROTON cv + + - - + + + 95/50 1M 37C sref: reference peak not found default calibration done
7 17:25:26 cv.200806.a400 20 PROTON cv + + - - + + + CV064 Chtipharm S Atto665 sref: reference peak not found default calibration done
6 17:09:22 cv.200806.a400 10 PROTON cv + + - + + + + MT02 95/5 Atto 665 sref: reference peak not found default calibration done
22 17:03:34 mci89.200806.a400 22 COSY mci - + - - - + +
22 16:27:47 mci89.200806.a400 21 C13 mci + + - + + + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
21 16:21:17 ap.200806.a400 22 F19CPD_KU ap + + - + + + + 6-89_2nd Rev blind_F1
19 15:58:30 at5_9_3fr44.200806.a400 11 PROTON at - + - - - + +
19 15:51:11 at5_9_3fr44.200806.a400 10 PROTON at + + - + + + +
22 15:28:36 mci89.200806.a400 20 PROTON mci + + - + + + + sref: reference peak not found default calibration done
21 15:25:48 ap.200806.a400 21 P31CPD ap - + - - - + + 6-89_2nd Rev blind_F1
21 15:15:12 ap.200806.a400 20 PROTON ap + + - + + + + 6-89_2nd Rev blind_F1
10 14:53:46 fm.200806.a400Fab29 11 C13 fm - + - - - + + Fab29 CDCl3 13C 06/08/20 au_zg_max30min: --- au_zg_max30min finished ---
10 14:46:52 fm.200806.a400Fab29 10 PROTON fm + + - - + + + Fab29 CDCl3 1H 06/08/20
9 14:30:51 fm.200806.a400Fab28 11 C13 fm - + - - - + + Fab28 CDCl3 13C 06/08/20 au_zg_max30min: --- au_zg_max30min finished ---
9 14:23:18 fm.200806.a400Fab28 10 PROTON fm + + - + + + + Fab28 CDCl3 1H 06/08/20
16 14:12:29 ktt.200806.a400 10 PROTON ktt + + - + + + + KTT15-92_recov
13 14:04:21 av.200806.a400 10 PROTON av + + - + + + + AV1-79
2 13:50:07 pd.200806.a400 11 P31CPD pd - + - - - + + PD-232A
2 13:39:23 pd.200806.a400 10 PROTON pd + + - + + + + PD-232A
1 12:55:45 ed.200806.a400 10 PROTON ed + + - + + + + Emil - Test reaction, methyl esterfication
8 12:18:34 bhg686_I.200806.a400 12 HSQC bhg - + - - - + +
8 12:02:47 bhg686_I.200806.a400 13 C13 bhg - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
8 11:57:00 bhg686_I.200806.a400 11 COSY bhg - + - - - + +
8 11:50:52 bhg686_I.200806.a400 10 PROTON bhg + + - + + + + sref: reference peak not found default calibration done
4 11:12:07 fr.200806.a400 10 PROTON fr + + - + + + + FR-102-1A
15 09:54:57 ap.200806.a400 11 P31CPD ap - + - - - + + NYR-4 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200806.a400/11/pdata/1/peaks!
15 09:48:32 ap.200806.a400 10 PROTON ap + + - + + + + NYR-4 sref: reference peak not found default calibration done
5 09:29:33 ki513_2ny.200806.a400 10 PROTON ki + + - + + + + KI 513-2 sref: reference peak not found default calibration done
22 02:42:07 ap.200805.a400 150 PROTON ap + + - - + + + 6-89_prep HPLC blind_2-3min
21 02:31:32 ap.200805.a400 140 PROTON ap + + - - + + + 6-89_prep HPLC blind_9-10min sref: reference peak not found default calibration done
24 02:20:36 ap.200805.a400 130 PROTON ap + + - - + + + 6-89 prep HPLC blind_3-4min
17 02:03:53 ap.200805.a400 120 PROTON ap + + - - + + + 6-89_prep HPLC blind_8-9min
18 01:18:11 cbc.200805.a400 15 HMBC cbc - + - - - + + CBC141 prep
18 00:09:11 cbc.200805.a400 14 C13CPD cbc + + - + + + + CBC141 prep sref: reference peak not found default calibration done
8 23:04:45 ktt.200805.a400 43 C13CPD ktt + + - - + + + KTT15-96_pur sref: reference peak not found default calibration done
7 22:00:05 ktt.200805.a400 13 C13CPD ktt + + - + + + + KTT15-94_pur sref: reference peak not found default calibration done
17 21:14:46 ap.200805.a400 110 PROTON ap + + - - + + + 6-89_prep HPLC blind_6-7min sref: reference peak not found default calibration done
9 20:58:07 ap.200805.a400 100 PROTON ap + + - + + + + 6-89_prep HPLC blind_4-5min
12 20:26:06 ap.200805.a400 90 PROTON ap + + - - + + + 6-89_prep HPLC blind_7-8min sref: reference peak not found default calibration done
11 20:15:19 ap.200805.a400 80 PROTON ap + + - + + + + 6-89_prep HPLC_blind_5-6min sref: reference peak not found default calibration done
8 18:56:46 ktt.200805.a400 42 HSQC ktt + + - - + + + KTT15-96_pur
7 18:35:59 ktt.200805.a400 12 HSQC ktt + + - + + + + KTT15-94_pur
18 18:15:19 cbc.200805.a400 13 HSQC cbc + + - + + + + CBC141 prep
20 18:06:42 gb.200805.a400 40 PROTON gb + + - + + + + GB-7-1
2 17:59:36 gb.200805.a400 30 PROTON gb + + - + + + + GB-7-1 sref: reference peak not found default calibration done
18 17:56:49 cbc.200805.a400 12 F19CPD_KU cbc - + - - - + + CBC141 prep
18 17:51:00 cbc.200805.a400 11 COSY cbc - + - - - + + CBC141 prep
18 17:39:51 cbc.200805.a400 10 PROTON cbc + + - + + + + CBC141 prep
8 17:34:04 ktt.200805.a400 41 COSY ktt - + - - - + + KTT15-96_pur
8 17:27:31 ktt.200805.a400 40 PROTON ktt + + - - + + + KTT15-96_pur sref: reference peak not found default calibration done
7 17:21:44 ktt.200805.a400 11 COSY ktt - + - - - + + KTT15-94_pur
7 17:14:58 ktt.200805.a400 10 PROTON ktt + + - + + + + KTT15-94_pur sref: reference peak not found default calibration done
1 17:02:45 ed.200805.a400 10 PROTON ed + + - + + + + emil - acid intermediate
6 16:46:11 jop.200805.a400 141 C13 jop - + - - - + + jop_IV_197_1 zg: DRU warning: One ADC-overflow received during acquisition (DRU 1)! For further details please have a look at the log-file E:/current_data/data/jop/nmr/jop.200805.a400/141/overflow_log_dru1.txt; au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
6 16:39:38 jop.200805.a400 140 PROTON jop + + - + + + + jop_IV_197_1 sref: reference peak not found default calibration done
13 16:31:56 jop.200805.a400 131 P31CPD jop - + - - - + + DAD040 F24 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/131/pdata/1/peaks!
13 16:25:15 jop.200805.a400 130 P31 jop + + - - + + + DAD040 F24 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/130/pdata/1/peaks!
12 16:23:20 jop.200805.a400 121 P31CPD jop - + - - - + + DAD040 F19 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/121/pdata/1/peaks!
12 16:17:07 jop.200805.a400 120 P31 jop + + - - + + + DAD040 F19 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/120/pdata/1/peaks!
11 16:15:12 jop.200805.a400 111 P31CPD jop - + - - - + + DAD040 F16 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/111/pdata/1/peaks!
11 16:08:45 jop.200805.a400 110 P31 jop + + - - + + + DAD040 F16 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/110/pdata/1/peaks!
10 16:06:43 jop.200805.a400 101 P31CPD jop - + - - - + + DAD040 F11 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/101/pdata/1/peaks!
10 15:59:58 jop.200805.a400 100 P31 jop + + - + + + + DAD040 F11 2 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/100/pdata/1/peaks!
19 15:35:26 at2_63.200805.a400 10 F19CPD_KU at + + - - + + +
16 15:27:30 gb.200805.a400 20 PROTON gb + + - - + + + GB-7-1
6 15:11:39 jop.200805.a400 91 C13 jop - + - - - + + JOP_IV_197_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
6 15:05:21 jop.200805.a400 90 PROTON jop + + - - x + + JOP_IV_197_1 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
15 14:58:36 jn51antcru.200805.a400 10 PROTON jn + + - - + + + jn51antcru sref: reference peak not found default calibration done
14 14:53:08 jn51f9_11.200805.a400 10 PROTON jn + + - - x + + jn51f9_11 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
23 14:46:10 jn51f65_70.200805.a400 10 PROTON jn + + - - + + + jn51f65_70 sref: reference peak not found default calibration done
22 14:41:13 jn51f41_46.200805.a400 10 PROTON jn + + - - x + + jn51f41_46 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
21 14:33:34 jn51antalk.200805.a400 10 PROTON jn + + - + + + + jn51antalk sref: reference peak not found default calibration done
13 14:27:29 jop.200805.a400 80 P31 jop + + - - + + + DAD040 F24 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/80/pdata/1/peaks!
12 14:21:09 jop.200805.a400 70 P31 jop + + - - + + + DAD040 F19 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/70/pdata/1/peaks!
11 14:14:45 jop.200805.a400 60 P31 jop + + - - + + + DAD040 F16 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/60/pdata/1/peaks!
10 14:07:18 jop.200805.a400 50 P31 jop + + - + + + + DAD040 F11 pp: Cannot find any peak for scaling in E:/current_data/data/jop/nmr/jop.200805.a400/50/pdata/1/peaks!
3 13:59:32 gb.200805.a400 10 PROTON gb + + - + + + + GB-7-1
9 13:57:18 pd.200805.a400 11 P31CPD pd - + - - - + + PD-232-CR
9 13:46:36 pd.200805.a400 10 PROTON pd + + - - + + + PD-232-CR
7 13:38:36 ap.200805.a400 70 PROTON ap + + - - + + + 6-89_2nd blind Rev_f21 sref: reference peak not found default calibration done
8 13:27:53 ap.200805.a400 60 PROTON ap + + - - + + + 6-89_2nd blind Rev_f14 sref: reference peak not found default calibration done
20 13:24:42 ap.200805.a400 52 F19CPD_KU ap - + - - - + + 6-89_2nd blind Rev_overnight rt
20 13:16:53 ap.200805.a400 51 P31CPD ap + + - - + + + 6-89_2nd blind Rev_overnight rt
19 13:14:51 ap.200805.a400 42 P31CPD ap - + - - - + + 6-89_2nd blind Rev_f19_overnight freezer
19 13:01:10 ap.200805.a400 41 F19CPD_KU ap + + - + + + + 6-89_2nd blind Rev_f19_overnight freezer
5 12:45:27 jop.200805.a400 41 C13 jop - + - - - + + jop_iv_196_1 au_zg_max30min: --- au_zg_max30min finished ---
5 12:38:19 jop.200805.a400 40 PROTON jop + + - - + + + jop_iv_196_1
4 12:22:17 jop.200805.a400 31 C13 jop - + - - - + + JOP_IV_195_1 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
4 12:15:02 jop.200805.a400 30 PROTON jop + + - + + + + JOP_IV_195_1
20 12:04:51 ap.200805.a400 50 PROTON ap + + - - + + + 6-89_2nd blind Rev_overnight rt sref: reference peak not found default calibration done
19 11:54:21 ap.200805.a400 40 PROTON ap + + - - + + + 6-89_2nd blind Rev_f19_overnight freezer sref: reference peak not found default calibration done
18 11:51:45 ap.200805.a400 31 P31CPD ap - + - - - + + 6-89_2nd blind Rev_f18
18 11:41:16 ap.200805.a400 30 PROTON ap + + - - + + + 6-89_2nd blind Rev_f18 sref: reference peak not found default calibration done
17 11:32:49 ap.200805.a400 21 P31CPD ap + + - + + + + 6-89_2nd blind Rev_f17
17 10:38:06 ap.200805.a400 20 PROTON ap + + - - + + + 6-89_2nd blind Rev_f17 sref: reference peak not found default calibration done, Automation was stopped
15 10:29:45 ap.200805.a400 10 PROTON ap + + - + + + + 6-89_2nd blind Rev_f15 sref: reference peak not found default calibration done
2 10:14:00 jop.200805.a400 21 C13 jop - + - - - + + DAD039 Br au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
2 10:07:01 jop.200805.a400 20 PROTON jop + + - - + + + DAD039 Br
1 09:51:06 jop.200805.a400 11 C13 jop - + - - - + + DAD035 Br au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 09:43:46 jop.200805.a400 10 PROTON jop + + - + + + + DAD035 Br
10 09:30:25 asma.200805.a400 10 PROTON asma + + - + + + + AM2-76 sref: reference peak not found default calibration done
16 21:26:29 ap.200804.a400 101 P31CPD ap - + - - - + + 6-89_2nd blind Rev_f20
16 21:15:40 ap.200804.a400 100 PROTON ap + + - - + + + 6-89_2nd blind Rev_f20 sref: reference peak not found default calibration done
17 21:05:16 ap.200804.a400 90 PROTON ap + + - + + + + 6-89_2nd blind Rev_f16 sref: reference peak not found default calibration done
12 20:48:07 ap.200804.a400 80 PROTON ap + + - + + + + 6-89_2nd blind Rev_f7 sref: reference peak not found default calibration done
21 20:39:33 ap.200804.a400 71 P31CPD ap - + - - - + + 6-89_2nd blind Rev_f21
21 20:29:19 ap.200804.a400 70 PROTON ap + + - - + + + 6-89_2nd blind Rev_f21
19 20:26:31 ap.200804.a400 61 P31CPD ap - + - - - + + 6-89_2nd blind Rev_f19
19 20:15:53 ap.200804.a400 60 PROTON ap + + - + + + + 6-89_2nd blind Rev_f19 sref: reference peak not found default calibration done
15 19:36:03 mci88.200804.a400 23 HSQC mci - + - - - + +
15 19:25:28 mci88.200804.a400 22 COSY mci + + - - + + +
11 19:18:17 yd.200804.a400 40 PROTON yd + + - + + + + YD-511-183-crude
10 18:47:54 cv.200804.a400 90 PROTON cv + + - - + + + Stability LA 110 Su 55 1M 4C sref: reference peak not found default calibration done
9 18:37:18 cv.200804.a400 80 PROTON cv + + - - + + + Stability LA 110 Su 55 1M RT sref: reference peak not found default calibration done
8 18:26:48 cv.200804.a400 70 PROTON cv + + - - + + + Stability LA 110 Su 55 1M 37 sref: reference peak not found default calibration done
7 18:15:10 cv.200804.a400 60 PROTON cv + + - + + + + Stability LA 32.5 1M 4C sref: reference peak not found default calibration done
15 17:59:26 mci88.200804.a400 21 C13 mci - + - - - + + au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
15 17:51:55 mci88.200804.a400 20 PROTON mci + + - + + + + sref: reference peak not found default calibration done
5 17:41:16 cv.200804.a400 50 PROTON cv + + - - + + + Stability LA 32.5 1M RT sref: reference peak not found default calibration done
4 17:30:20 cv.200804.a400 40 PROTON cv + + - + + + + Stability LA 32.5 1M 37C sref: reference peak not found default calibration done
24 17:26:05 par.200804.a400 20 PROTON par + + - x - - - 100-008-crude-again Lock failed after multiple attempts, lock: Command 'lock CDCl3' failed. Lock is OFF, Command 'lock CDCl3' failed. Lock is OFF
14 17:15:20 ap.200804.a400 50 PROTON ap + + - + + + + 6-89_f13,14
3 17:05:22 cv.200804.a400 30 PROTON cv + + - - + + + CO 212-191018-01 sref: reference peak not found default calibration done
2 16:53:42 cv.200804.a400 20 PROTON cv + + - + + + + CO 212-060516-01 sref: reference peak not found default calibration done
12 16:35:22 mci87repur.200804.a400 20 C13 mci + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
11 16:27:57 mci88.200804.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
1 16:11:34 cv.200804.a400 10 PROTON cv + + - + + + + CV063 95/50 atto665 sref: reference peak not found default calibration done
6 16:04:11 par.200804.a400 10 PROTON par + + - - + + + 100-007-crude-before filteration
11 15:52:52 mci87repur.200804.a400 11 COSY mci + + - - + + +
20 15:45:18 cvh.200804.a400 30 PROTON cvh + + - - + + + CVI1-45 5-11
5 15:38:19 gb.200804.a400 10 PROTON gb + + - + + + + GB-7-1
17 14:54:53 ye_40M_1.200804.a400 10 PROTON ye + + - - + + + sref: reference peak not found default calibration done
16 14:47:56 cvh.200804.a400 20 PROTON cvh + + - + + + + CVI1-43 4-8
14 14:41:50 yd.200804.a400 30 PROTON yd + + - + + + + YD-601-181-crude sref: reference peak not found default calibration done
13 14:35:18 yd.200804.a400 20 PROTON yd + + - + + + + YD-607-179 sref: reference peak not found default calibration done
12 14:26:05 em1027.200804.a400 10 PROTON emr + + - - + + +
11 14:18:45 mci87repur.200804.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
7 12:50:17 cyl.200804.a400 23 HSQCETGP cyl + + - + + + + mcd_cl-02-21
18 12:41:47 ap.200804.a400 40 P31CPD ap + + - + + + + 6-89_f8
12 12:34:28 cvh.200804.a400 10 PROTON cvh + + - + + + + CVI1-45 Fraction 5-11
8 12:27:55 yd.200804.a400 10 PROTON yd + + - - x + + YD-510-180-pure topshim: PerformShimming - too many points lost during fit, Shim failed, sref: reference peak not found default calibration done
7 12:22:06 cyl.200804.a400 22 COSY cyl - + - - - + + mcd_cl-02-21
7 12:06:02 cyl.200804.a400 21 C13 cyl - + - - - + + mcd_cl-02-21 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
7 11:59:24 cyl.200804.a400 20 PROTON cyl + + - + + + + mcd_cl-02-21 sref: reference peak not found default calibration done
4 11:44:21 fr.200804.a400 30 PROTON fr + + - + + + + para-tol boronic acid
3 11:37:54 cyl.200804.a400 10 PROTON cyl + + - + + + + MCD_CL02-21 sref: reference peak not found default calibration done
1 11:29:06 ed.200804.a400 10 PROTON ed + + - - + + + Emil - ED Acid intermediate
6 11:23:03 fr.200804.a400 20 PROTON fr x - - - - - - para-tol-boronic acid Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 6
5 11:15:48 fr.200804.a400 10 PROTON fr + + - + + + + 3-Br-SPh-indole
9 10:50:14 ap.200804.a400 31 F19CPD_KU ap - + - - - + + carnitine BF4-
9 10:43:32 ap.200804.a400 30 PROTON ap + + - - + + + carnitine BF4- sref: reference peak not found default calibration done
10 10:36:26 ap.200804.a400 20 PROTON ap + + - + + + + carnitine zwitterion after H2O f drying sref: reference peak not found default calibration done
17 10:20:22 av.200804.a400 20 PROTON av + + - + + + + AV1-77
14 10:12:29 ap.200804.a400 11 F19CPD_KU ap - + - - - + + 6-89_f6,7
14 10:05:12 ap.200804.a400 10 P31CPD ap + + - + + + + 6-89_f6,7
2 09:55:56 av.200804.a400 10 PROTON av + + - + + + + AV1-77 27-30
1 08:44:30 asma.200804.a400 10 PROTON asma + + - + + + + AM2-74-2 sref: reference peak not found default calibration done
19 23:07:27 atfr86.200803.a400 11 C13CPD at + + - + + + +
15 22:02:12 bhg670_I.200803.a400 13 C13CPD bhg + + - + + + + sref: reference peak not found default calibration done
19 21:46:06 atfr86.200803.a400 10 PROTON at + + - + + + +
12 21:31:37 ap.200803.a400 90 PROTON ap + + - - + + + 6-89_f11 sref: reference peak not found default calibration done
9 21:20:40 ap.200803.a400 80 PROTON ap + + - - + + + 6-89_f6,7 sref: reference peak not found default calibration done
10 21:10:49 ap.200803.a400 70 PROTON ap + + - - + + + 6-89_f4,5 sref: reference peak not found default calibration done
7 21:00:16 ap.200803.a400 60 PROTON ap + + - - + + + 6-89_f10 sref: reference peak not found default calibration done
8 20:49:21 ap.200803.a400 50 PROTON ap + + - - + + + 6-89_f9 sref: reference peak not found default calibration done
9 20:38:06 ap.200803.a400 40 PROTON ap + + - + + + + 6-89_f8 sref: reference peak not found default calibration done
10 20:26:56 ap.200803.a400 30 PROTON ap + + - + + + + 6-89_f6,7 sref: reference peak not found default calibration done
17 19:16:18 av.200803.a400 20 PROTON av + + - - + + + AV1-77 fr25 sref: reference peak not found default calibration done
13 18:48:20 em.200803.a400 11 PROTON em + + - + + + + 135rec_conc
13 18:10:52 em.200803.a400 10 PROTON em + + - + + + + 135rec
8 17:28:34 cbc.200803.a400 10 PROTON cbc + + - + + + + CBC141 crude
5 16:50:43 cvh.200803.a400 30 PROTON cvh + + - + + + + cvi1-42 19-23 sref: reference peak not found default calibration done
18 16:29:10 mci87new.200803.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
23 15:56:53 yd.200803.a400 11 PROTON yd - + - - - + + YD-607-179-crude-water extraction for the second time sref: reference peak not found default calibration done
23 15:50:53 yd.200803.a400 10 PROTON yd + + - + + + + YD-607-179-crude-water extraction for the second time sref: reference peak not found default calibration done
22 15:31:27 asma.200803.a400 11 C13 asma - + - - - + + AM2-76 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
22 15:23:49 asma.200803.a400 10 PROTON asma + + - + + + + AM2-76 sref: reference peak not found default calibration done
2 14:13:45 pd.200803.a400 11 P31CPD pd - + - - - + + PD-230A
2 14:03:00 pd.200803.a400 10 PROTON pd + + - + + + + PD-230A
24 13:45:38 atf27.200803.a400 10 PROTON at + + - - + + +
14 13:38:29 atf14.200803.a400 10 PROTON at + + - - + + +
11 13:30:56 atf1.200803.a400 10 PROTON at + + - + + + + sref: reference peak not found default calibration done
17 12:14:50 av.200803.a400 11 HSQC av - + - - - + +
17 12:07:51 av.200803.a400 10 PROTON av + + - + + + +
15 11:20:27 bhg670_I.200803.a400 12 HSQC bhg - + - - - + +
15 11:14:35 bhg670_I.200803.a400 11 COSY bhg - + - - - + +
15 11:07:15 bhg670_I.200803.a400 10 PROTON bhg + + - + + + +
10 11:00:02 cvh.200803.a400 20 PROTON cvh + + - + + + + cvi1-42 11
1 10:44:24 fm.200803.a400Fab25 11 C13 fm - + - - - + + Fab25_prove CDCl3 13C 03/07/20 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
1 10:37:07 fm.200803.a400Fab25 10 PROTON fm + + - + + + + Fab25_prove CDCl3 1H 03/07/20
6 10:13:32 ap.200803.a400 23 HSQC ap + + - - + + + 7-2_2nd prep HPLC_F1
7 09:54:17 ap.200803.a400 13 HSQC ap + + - - + + + 7-2_2nd prep HPLC_F2
6 09:52:03 ap.200803.a400 22 F19CPD_KU ap - + - - - + + 7-2_2nd prep HPLC_F1
6 09:50:00 ap.200803.a400 21 P31CPD ap - + - - - + + 7-2_2nd prep HPLC_F1
6 09:38:33 ap.200803.a400 20 PROTON ap + + - + + + + 7-2_2nd prep HPLC_F1 sref: reference peak not found default calibration done
11 09:31:11 cvh.200803.a400 10 PROTON cvh + + - + + + + cvi1-44
7 09:28:51 ap.200803.a400 12 F19CPD_KU ap - + - - - + + 7-2_2nd prep HPLC_F2
7 09:26:43 ap.200803.a400 11 P31CPD ap - + - - - + + 7-2_2nd prep HPLC_F2
7 09:16:07 ap.200803.a400 10 PROTON ap + + - + + + + 7-2_2nd prep HPLC_F2 sref: reference peak not found default calibration done
14 23:04:21 ap.200801.a400 34 C13CPD ap + + - - + + + 7-2_1st prep HPLC_F2 sref: reference peak not found default calibration done
19 22:00:15 ap.200801.a400 24 C13CPD ap + + - + + + + 7-2_1st prep HPLC_F1 sref: reference peak not found default calibration done
14 19:03:49 ap.200801.a400 33 HSQC ap + + - - + + + 7-2_1st prep HPLC_F2
19 18:44:32 ap.200801.a400 23 HSQC ap + + - - + + + 7-2_1st prep HPLC_F1
14 18:42:18 ap.200801.a400 32 F19CPD_KU ap - + - - - + + 7-2_1st prep HPLC_F2
14 18:40:13 ap.200801.a400 31 P31CPD ap - + - - - + + 7-2_1st prep HPLC_F2
14 18:29:34 ap.200801.a400 30 PROTON ap + + - - + + + 7-2_1st prep HPLC_F2 sref: reference peak not found default calibration done
19 18:27:14 ap.200801.a400 22 F19CPD_KU ap - + - - - + + 7-2_1st prep HPLC_F1
19 18:25:05 ap.200801.a400 21 P31CPD ap - + - - - + + 7-2_1st prep HPLC_F1
19 18:14:21 ap.200801.a400 20 PROTON ap + + - + + + + 7-2_1st prep HPLC_F1 sref: reference peak not found default calibration done
6 16:55:10 mci87f6369.200801.a400 10 PROTON mci + + - - + + +
5 16:47:44 mci87f1349.200801.a400 10 PROTON mci + + - + + + + sref: reference peak not found default calibration done
16 15:11:40 ap.200801.a400 12 HSQC ap - + - - - + + 7-4
16 15:09:31 ap.200801.a400 11 P31CPD ap - + - - - + + 7-4 pp: Cannot find any peak for scaling in E:/current_data/data/ap/nmr/ap.200801.a400/11/pdata/1/peaks!
16 14:58:35 ap.200801.a400 10 PROTON ap + + - + + + + 7-4 sref: reference peak not found default calibration done
18 14:19:23 yst.200801.a400 10 PROTON yst + + - + + + + YST-271
19 02:45:12 ap.200731.a400 34 C13CPD ap - + - - - + + 7-3 sref: reference peak not found default calibration done
19 02:29:30 ap.200731.a400 33 HSQC ap - + - - - + + 7-3
19 02:27:10 ap.200731.a400 32 F19CPD_KU ap - + - - - + + 7-3
19 02:20:23 ap.200731.a400 31 P31CPD ap + + - + + + + 7-3
20 01:28:57 at.200731.a400 13 HMBC_LP at + + - + + + +
23 00:24:03 ap.200731.a400 21 C13CPD ap + + - + + + + sref: reference peak not found default calibration done
15 23:21:25 jmr.200731.a400 11 C13CPD jmr + + - - x + + topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed, sref: reference peak not found default calibration done
12 23:06:12 emr.200731.a400 12 HSQCETGP emr - + - - - + + jn235
12 22:00:49 emr.200731.a400 11 C13CPD emr + + - + + + + jn235 sref: reference peak not found default calibration done
19 21:49:45 ap.200731.a400 30 PROTON ap + + - + + + + 7-3 sref: reference peak not found default calibration done
9 21:11:04 av.200731.a400 30 PROTON av + + - + + + + AV1-76 46 49 sref: reference peak not found default calibration done
8 20:22:11 yst.200731.a400 20 PROTON yst + + - + + + + YST-270-2
6 20:16:19 gg.200731.a400 20 PROTON gg + + - - + + + GG01-22P sref: reference peak not found default calibration done
5 20:09:41 gg.200731.a400 10 PROTON gg + + - + + + + GG01-09.1 sref: reference peak not found default calibration done
1 19:27:16 pd.200731.a400 40 PROTON pd + + - - + + + PD-226A_Recov Alkene sref: reference peak not found default calibration done
24 19:24:49 pd.200731.a400 31 F19CPD_KU pd - + - - - + + PD-225A
24 19:18:17 pd.200731.a400 30 PROTON pd + + - - + + + PD-225A
22 19:15:24 pd.200731.a400 21 P31CPD pd - + - - - + + PD-228-CR
22 19:07:30 pd.200731.a400 20 PROTON pd + + - + + + + PD-228-CR sref: reference peak not found default calibration done
20 18:17:50 at.200731.a400 12 HSQC at - + - - - + +
20 18:12:06 at.200731.a400 11 COSY at - + - - - + +
20 18:04:57 at.200731.a400 10 PROTON at + + - - + + +
10 17:57:47 cvh.200731.a400 10 PROTON cvh + + - - + + + cvi1-42 sref: reference peak not found default calibration done
18 17:22:25 av.200731.a400 11 C13 av + + - + + + + AV1-76 38 41 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
23 17:11:47 ap.200731.a400 20 PROTON ap + + - + + + + carnitine zwitterion sref: reference peak not found default calibration done
19 17:00:56 av.200731.a400 20 PROTON av + + - - + + + AV1-76 35 37 double spot sref: reference peak not found default calibration done
18 16:54:02 av.200731.a400 10 PROTON av + + - + + + + AV1-76 38 41 sref: reference peak not found default calibration done
15 16:28:39 jmr.200731.a400 10 PROTON jmr + + - + + + +
2 16:20:04 yst.200731.a400 10 PROTON yst + + - + + + + YST-269-3
24 16:07:43 rr.200731.a400 180 PROTON rr + + - - + + + Aze141
23 16:01:55 rr.200731.a400 170 PROTON rr + + - - + + + Aze140
22 15:56:05 rr.200731.a400 160 PROTON rr + + - - + + + Aze139
21 15:50:04 rr.200731.a400 150 PROTON rr + + - - + + + Aze137
20 15:44:01 rr.200731.a400 140 PROTON rr + + - - + + + Aze136
19 15:38:06 rr.200731.a400 130 PROTON rr + + - - + + + Aze135
18 15:31:32 rr.200731.a400 120 PROTON rr + + - + + + + Aze134
16 15:28:57 umb399.200731.a400 11 F19CPD_KU umb - + - - - + +
16 15:22:28 umb399.200731.a400 10 PROTON umb + + - + + + +
11 15:11:41 rr.200731.a400 110 PROTON rr + + - - + + + Aze133
10 15:05:47 rr.200731.a400 100 PROTON rr + + - - + + + Aze132
9 14:59:47 rr.200731.a400 90 PROTON rr + + - - + + + Aze131
8 14:53:55 rr.200731.a400 80 PROTON rr + + - - + + + Aze130
7 14:46:38 rr.200731.a400 70 PROTON rr + + - + + + + Aze129
13 14:26:02 emr.200731.a400 22 HSQCETGP emr + + - + + + + 1021
17 14:19:56 emr.200731.a400 30 PROTON emr + + - - + + + 1021 dmso sref: reference peak not found default calibration done
6 14:13:52 rr.200731.a400 60 PROTON rr + + - - + + + Aze128
5 14:06:32 rr.200731.a400 50 PROTON rr + + - + + + + Aze118
13 13:50:42 emr.200731.a400 21 C13 emr - + - - - + + 1021 au_zg_max30min: --- au_zg_max30min finished ---, sref: reference peak not found default calibration done
13 13:46:00 emr.200731.a400 20 PROTON emr + + - - x + + 1021 topshim: PrepareLock - lock is pending: please lock in prior to shimming, Shim failed
12 13:38:30 emr.200731.a400 10 PROTON emr + + - + + + + jn235
4 13:32:26 rr.200731.a400 40 PROTON rr + + - - + + + Aze113
3 13:26:21 rr.200731.a400 30 PROTON rr + + - - + + + Aze112
2 13:20:17 rr.200731.a400 20 PROTON rr + + - - + + + Aze111
1 13:13:37 rr.200731.a400 10 PROTON rr + + - + + + + Aze110